N-{7-[(2E)-3-(2,6-dichlorophenyl)prop-2-enoyl]-2,3-dimethylimidazo[1,2-a]pyridin-8-yl}-2,2-dimethylpropanamide

Base Information

• Chemical Name: N-{7-[(2E)-3-(2,6-dichlorophenyl)prop-2-enoyl]-2,3-dimethylimidazo[1,2-a]pyridin-8-yl}-2,2-dimethylpropanamide
• CAS No.: 1092480-04-0
• Molecular Formula: C₂₃H₂₃Cl₂N₃O₂
• Molecular Weight: 444.361

Synonyms:N-{7-[(2E)-3-(2,6-dichlorophenyl)prop-2-enoyl]-2,3-dimethylimidazo[1,2-a]pyridin-8-yl}-2,2-dimethylpropanamide

Chemical Property of N-{7-[(2E)-3-(2,6-dichlorophenyl)prop-2-enoyl]-2,3-dimethylimidazo[1,2-a]pyridin-8-yl}-2,2-dimethylpropanamide

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Technology Process of N-{7-[(2E)-3-(2,6-dichlorophenyl)prop-2-enoyl]-2,3-dimethylimidazo[1,2-a]pyridin-8-yl}-2,2-dimethylpropanamide

There total 1 articles about N-{7-[(2E)-3-(2,6-dichlorophenyl)prop-2-enoyl]-2,3-dimethylimidazo[1,2-a]pyridin-8-yl}-2,2-dimethylpropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-[2,3-dimethyl-7-(tributylstannyl)imidazo[1,2-a]pyridin-8-yl]-2,2-dimethylpropanamide + 3-(2,6-dichloro-phenyl)-acryloyl chloride (52479-64-8,230305-41-6) → N-{7-[(2E)-3-(2,6-dichlorophenyl)prop-2-enoyl]-2,3-dimethylimidazo[1,2-a]pyridin-8-yl}-2,2-dimethylpropanamide (1092480-04-0)

Guidance literature:

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; lithium chloride; In tetrahydrofuran; at 60 ℃;

DOI:10.1055/s-2008-1067264

Reference yield: 41.0%

N-{7-[(2E)-3-(2,6-dichlorophenyl)prop-2-enoyl]-2,3-dimethylimidazo[1,2-a]pyridin-8-yl}-2,2-dimethylpropanamide (1092480-04-0) → 9-(2,6-dichlorophenyl)-2,3-dimethyl-9,10-dihydroimidazo[1,2-h]-1,7-naphthyridin-7(8H)-one

Guidance literature:

With sulfuric acid; In 1,4-dioxane; water; at 100 ℃;

DOI:10.1055/s-2008-1067264

upstream raw materials:

3-(2,6-dichloro-phenyl)-acryloyl chloride

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