methyl 3-methoxycarbonyl-5-(2,6,6-trimethyl-2-cyclohexenyl)-3-pentenoate

Base Information

Chemical Name:methyl 3-methoxycarbonyl-5-(2,6,6-trimethyl-2-cyclohexenyl)-3-pentenoate
CAS No.:143658-46-2
Molecular Formula:C₁₇H₂₆O₄
Molecular Weight:294.391
Hs Code.:

Synonyms:methyl 3-methoxycarbonyl-5-(2,6,6-trimethyl-2-cyclohexenyl)-3-pentenoate

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Chemical Property of methyl 3-methoxycarbonyl-5-(2,6,6-trimethyl-2-cyclohexenyl)-3-pentenoate

Chemical Property:

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Technology Process of methyl 3-methoxycarbonyl-5-(2,6,6-trimethyl-2-cyclohexenyl)-3-pentenoate

There total 4 articles about methyl 3-methoxycarbonyl-5-(2,6,6-trimethyl-2-cyclohexenyl)-3-pentenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 143658-45-1
2-(2,6,6-trimethyl-2-cyclohexenyl)ethanal

: 1104-78-5
dimethyl 2-(triphenylphosphoranylidene)succinate

: 143658-46-2
methyl 3-methoxycarbonyl-5-(2,6,6-trimethyl-2-cyclohexenyl)-3-pentenoate

Guidance literature:: In benzene; for 11h; Heating;

Reference yield:

: 134780-16-8
(R)-2,4,4-trimethyl-2-cyclohexen-1-ol

: 143658-46-2
methyl 3-methoxycarbonyl-5-(2,6,6-trimethyl-2-cyclohexenyl)-3-pentenoate

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / propanoic acid / 59.5 h / 140 - 150 °C

2: 85 percent / LiAlH₄ / tetrahydrofuran / 16 h / 25 °C

3: 1.) oxalyl chloride, DMSO, 2.) Et₃N / 1.) CH₂Cl₂, -60 deg C, 30 min, 2.) CH₂Cl₂, from -60 deg C to 0 deg C, 1 h

4: 88 percent / benzene / 11 h / Heating

With lithium aluminium tetrahydride; oxalyl dichloride; dimethyl sulfoxide; propionic acid; triethylamine; In tetrahydrofuran; benzene;

Reference yield:

: 143658-43-9
ethyl <2,6,6-trimethyl-2-cyclohexenyl>acetate

: 143658-46-2
methyl 3-methoxycarbonyl-5-(2,6,6-trimethyl-2-cyclohexenyl)-3-pentenoate

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / LiAlH₄ / tetrahydrofuran / 16 h / 25 °C

2: 1.) oxalyl chloride, DMSO, 2.) Et₃N / 1.) CH₂Cl₂, -60 deg C, 30 min, 2.) CH₂Cl₂, from -60 deg C to 0 deg C, 1 h

3: 88 percent / benzene / 11 h / Heating

With lithium aluminium tetrahydride; oxalyl dichloride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; benzene;