N-(3-((1H-1,2,4-triazol-5-yl)thio)-4-hydroxyphenyl)-2,6-dichlorobenzenesulfonamide

Base Information

Chemical Name:N-(3-((1H-1,2,4-triazol-5-yl)thio)-4-hydroxyphenyl)-2,6-dichlorobenzenesulfonamide
CAS No.:1489231-00-6
Molecular Formula:C₁₄H₁₀Cl₂N₄O₃S₂
Molecular Weight:417.296
Hs Code.:

Synonyms:N-(3-((1H-1,2,4-triazol-5-yl)thio)-4-hydroxyphenyl)-2,6-dichlorobenzenesulfonamide

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Chemical Property of N-(3-((1H-1,2,4-triazol-5-yl)thio)-4-hydroxyphenyl)-2,6-dichlorobenzenesulfonamide

Chemical Property:

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Technology Process of N-(3-((1H-1,2,4-triazol-5-yl)thio)-4-hydroxyphenyl)-2,6-dichlorobenzenesulfonamide

There total 4 articles about N-(3-((1H-1,2,4-triazol-5-yl)thio)-4-hydroxyphenyl)-2,6-dichlorobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1489230-97-8
2,6-dichloro-N-(4-oxocyclohexa-2,5-dien-1-ylidene)benzenesulfonamide

: 3179-31-5
1H-1,2,4-triazole-5-thiol

: 1489231-00-6
N-(3-((1H-1,2,4-triazol-5-yl)thio)-4-hydroxyphenyl)-2,6-dichlorobenzenesulfonamide

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃; for 4h;
DOI:10.1016/j.ejmech.2013.07.056

Reference yield:

: 6579-54-0
2,6-dichlorobenzenesulfonyl chloride

: 1489231-00-6
N-(3-((1H-1,2,4-triazol-5-yl)thio)-4-hydroxyphenyl)-2,6-dichlorobenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 5 h / 20 °C / Cooling with ice

2: SiO₂-supported NaIO₄ / dichloromethane / 2 h / 20 °C

3: N,N-dimethyl-formamide / 4 h / 20 °C

With SiO₂-supported NaIO₄; In pyridine; dichloromethane; N,N-dimethyl-formamide; 3: |Michael Addition;
DOI:10.1016/j.ejmech.2013.07.056

Reference yield:

: 19818-15-6
2,6-dichloro-N-(4-hydroxyphenyl)benzenesulfonamide

: 1489231-00-6
N-(3-((1H-1,2,4-triazol-5-yl)thio)-4-hydroxyphenyl)-2,6-dichlorobenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: SiO₂-supported NaIO₄ / dichloromethane / 2 h / 20 °C

2: N,N-dimethyl-formamide / 4 h / 20 °C

With SiO₂-supported NaIO₄; In dichloromethane; N,N-dimethyl-formamide; 2: |Michael Addition;
DOI:10.1016/j.ejmech.2013.07.056