bis[(p-nitronyl nitroxide-phenyl)diphenylphosphine]dichloropalladium(II)

Base Information

Chemical Name:bis[(p-nitronyl nitroxide-phenyl)diphenylphosphine]dichloropalladium(II)
CAS No.:252933-18-9
Molecular Formula:C₅₀H₅₂Cl₂N₄O₄P₂Pd
Molecular Weight:1012.26
Hs Code.:

Synonyms:bis[(p-nitronyl nitroxide-phenyl)diphenylphosphine]dichloropalladium(II)

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Chemical Property of bis[(p-nitronyl nitroxide-phenyl)diphenylphosphine]dichloropalladium(II)

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Technology Process of bis[(p-nitronyl nitroxide-phenyl)diphenylphosphine]dichloropalladium(II)

There total 2 articles about bis[(p-nitronyl nitroxide-phenyl)diphenylphosphine]dichloropalladium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 252933-22-5
PdCl₂(P(C₆H₅)2(C₆H₄CH(NOH)2(C(CH₃)2)2))2

: 252933-18-9
bis[(p-nitronyl nitroxide-phenyl)diphenylphosphine]dichloropalladium(II)

Guidance literature:: With NaIO₄; In dichloromethane; water; N2-atmosphere; stirring (overnight); drying (MgSO4), evapn. (vac.), crystn. on slow CH2Cl2 / hexanes soln. evapn., drying (vac.); elem. anal.;
DOI:10.1021/om9905862

Reference yield: 53.0%

: 220778-21-2
[(p-(4,4,5,5-tetramethylimidazolinyl-1-oxyl-3-oxide)phenyl)diphenylphosphine]

: palladium dichloride

: 252933-18-9
bis[(p-nitronyl nitroxide-phenyl)diphenylphosphine]dichloropalladium(II)

Guidance literature:: In acetonitrile; N2-atmosphere; stirring (3 h); evapn. (vac.), crystn. on slow CH2Cl2 / hexanes evapn.; elem. anal.;
DOI:10.1021/om9905862