C₂₉H₂₆Cl₄O₆

Base Information

Chemical Name:C₂₉H₂₆Cl₄O₆
CAS No.:936338-10-2
Molecular Formula:C₂₉H₂₆Cl₄O₆
Molecular Weight:612.334
Hs Code.:

C<sub>29</sub>H<sub>26</sub>Cl<sub>4</sub>O<sub>6</sub>

Synonyms:C₂₉H₂₆Cl₄O₆

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Chemical Property of C₂₉H₂₆Cl₄O₆

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Technology Process of C₂₉H₂₆Cl₄O₆

There total 13 articles about C₂₉H₂₆Cl₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 936338-09-9
C₃₁H₃₂Cl₄O₆

: 936338-10-2
C₂₉H₂₆Cl₄O₆

Guidance literature:: With boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 0.166667h;
DOI:10.1021/jo0700474

Reference yield:

: C₂₈H₃₂Cl₄O₄

: 936338-10-2
C₂₉H₂₆Cl₄O₆

Guidance literature:: Multi-step reaction with 11 steps

1.1: (PCy₃)2Ru=CHPh / CH₂Cl₂ / 5 h / Heating

2.1: 3.50 g / lead(IV) acetate / CH₂Cl₂ / 20 °C

3.1: 53 percent / (-)-N-(1-phenylethyl)-1-azabicyclo[2.2.2]octan-3-amine; lithium chloride; n-butyllithium / tetrahydrofuran; hexane / 0.17 h / -78 °C

4.1: m-chloroperoxybenzoic acid / CH₂Cl₂ / 4 h / 20 °C

5.1: florisil / CH₂Cl₂ / 2 h

6.1: 4.90 g / IBX / dimethylsulfoxide / 1 h / 20 °C

7.1: 4.36 g / N,N-dimethylaniline / CH₂Cl₂ / -78 - 20 °C

8.1: 73 percent / tributyltin hydride; BEt₃; air / toluene; hexane / 0.5 h / 20 °C

9.1: N,N-diisopropylethylamine / CH₂Cl₂ / 4 h / -20 °C

10.1: CH₂Cl₂ / 3 h / 35 °C

10.2: 356 mg / 3-chloroperoxybenzoic acid / CH₂Cl₂ / 1 h / 20 °C

11.1: 78 percent / 3-chloroperoxybenzoic acid; BF₃*OEt₂ / CH₂Cl₂ / 0.17 h / 20 °C

With lead(IV) acetate; florisil; n-butyllithium; air; triethyl borane; boron trifluoride diethyl etherate; tri-n-butyl-tin hydride; N,N-dimethyl-aniline; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium chloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; (PCy₃)2Ru=CHPh; In tetrahydrofuran; hexane; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1021/jo0700474

Reference yield:

: 936338-30-6
C₂₆H₂₆Cl₄O₄

: 936338-10-2
C₂₉H₂₆Cl₄O₆

Guidance literature:: Multi-step reaction with 8 steps

1.1: m-chloroperoxybenzoic acid / CH₂Cl₂ / 4 h / 20 °C

2.1: florisil / CH₂Cl₂ / 2 h

3.1: 4.90 g / IBX / dimethylsulfoxide / 1 h / 20 °C

4.1: 4.36 g / N,N-dimethylaniline / CH₂Cl₂ / -78 - 20 °C

5.1: 73 percent / tributyltin hydride; BEt₃; air / toluene; hexane / 0.5 h / 20 °C

6.1: N,N-diisopropylethylamine / CH₂Cl₂ / 4 h / -20 °C

7.1: CH₂Cl₂ / 3 h / 35 °C

7.2: 356 mg / 3-chloroperoxybenzoic acid / CH₂Cl₂ / 1 h / 20 °C

8.1: 78 percent / 3-chloroperoxybenzoic acid; BF₃*OEt₂ / CH₂Cl₂ / 0.17 h / 20 °C

With florisil; air; triethyl borane; boron trifluoride diethyl etherate; tri-n-butyl-tin hydride; N,N-dimethyl-aniline; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In hexane; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1021/jo0700474