dimethyl (1α,2β,5β,6α)-9,9-diphenyl-3,4,7,8-tetrazatricyclo<4.3.0.0^2,5>non-7-ene-3,4-dicarboxylate

Base Information

• Chemical Name: dimethyl (1α,2β,5β,6α)-9,9-diphenyl-3,4,7,8-tetrazatricyclo<4.3.0.0^2,5>non-7-ene-3,4-dicarboxylate
• CAS No.: 105367-57-5
• Molecular Formula: C₂₁H₂₀N₄O₄
• Molecular Weight: 392.414

Synonyms:dimethyl (1α,2β,5β,6α)-9,9-diphenyl-3,4,7,8-tetrazatricyclo<4.3.0.0^2,5>non-7-ene-3,4-dicarboxylate

Chemical Property of dimethyl (1α,2β,5β,6α)-9,9-diphenyl-3,4,7,8-tetrazatricyclo<4.3.0.0^2,5>non-7-ene-3,4-dicarboxylate

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Technology Process of dimethyl (1α,2β,5β,6α)-9,9-diphenyl-3,4,7,8-tetrazatricyclo<4.3.0.0^2,5>non-7-ene-3,4-dicarboxylate

There total 1 articles about dimethyl (1α,2β,5β,6α)-9,9-diphenyl-3,4,7,8-tetrazatricyclo<4.3.0.0^2,5>non-7-ene-3,4-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3-diaza-bicyclo[2.2.0]hex-5-ene-2,3-dicarboxylic acid dimethyl ester (19839-41-9) + diazodiphenylmethane (908093-98-1) → dimethyl (1α,2β,5β,6α)-9,9-diphenyl-3,4,7,8-tetrazatricyclo<4.3.0.02,5>non-7-ene-3,4-dicarboxylate (105367-57-5)

Guidance literature:

DOI:10.1016/S0040-4039(00)99866-6

Reference yield: 95.0%

dimethyl (1α,2β,5β,6α)-9,9-diphenyl-3,4,7,8-tetrazatricyclo<4.3.0.02,5>non-7-ene-3,4-dicarboxylate (105367-57-5) → 1-((1S,2S,4R,5R)-7-Acetyl-3,3-diphenyl-6,7-diaza-tricyclo[3.2.0.02,4]hept-6-yl)-ethanone

Guidance literature:

In toluene; at 110 ℃;

DOI:10.1016/S0040-4039(00)99866-6

Reference yield: 95.0%

dimethyl (1α,2β,5β,6α)-9,9-diphenyl-3,4,7,8-tetrazatricyclo<4.3.0.02,5>non-7-ene-3,4-dicarboxylate (105367-57-5) → dimethyl (1α,2β,4β,5α)-3,3-diphenyl-6,7-diazatricyclo<3.2.0.02,4>heptane-6,7-dicarboxylate (105367-60-0)

Guidance literature:

In toluene; for 2h; Heating;

upstream raw materials:

2,3-diaza-bicyclo[2.2.0]hex-5-ene-2,3-dicarboxylic acid dimethyl ester

diazodiphenylmethane

Downstream raw materials:

dimethyl (1α,2β,4β,5α)-3,3-diphenyl-6,7-diazatricyclo<3.2.0.0^2,4>heptane-6,7-dicarboxylate

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