C₅₉H₇₆N₁₀O₉

Base Information

• Chemical Name: C₅₉H₇₆N₁₀O₉
• CAS No.: 170018-92-5
• Molecular Formula: C₅₉H₇₆N₁₀O₉
• Molecular Weight: 1069.31
• Mol file: 170018-92-5.mol

Synonyms:C₅₉H₇₆N₁₀O₉

Chemical Property of C₅₉H₇₆N₁₀O₉

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₉H₇₆N₁₀O₉

There total 11 articles about C₅₉H₇₆N₁₀O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-tert-butoxycarbonylamino-1-aminopentane (51644-96-3) → C59H76N10O9 (170018-92-5)

Guidance literature:

Multi-step reaction with 10 steps

1: 99 percent / NaBH₄, MgSO₄ / methanol

2: 79 percent / KF, celite / acetonitrile / 82 °C

3: NH₂NH₂ / methanol / 50 °C

4: NaBH₄, MgSO₄ / methanol

5: KF, celite / acetonitrile / 82 °C

6: NH₂NH₂ / methanol / 50 °C

7: 88 percent / CH₂Cl₂

8: TFA

9: TEA / CH₂Cl₂

10: TFA

With potassium fluoride; sodium tetrahydroborate; Celite; TEA; magnesium sulfate; trifluoroacetic acid; hydrazine; In methanol; dichloromethane; acetonitrile;

DOI:10.1016/S0040-4039(00)82310-2

Reference yield:

N1-benzyl-N5-(tert-butoxycarbonyl)-1,5-diaminopentane (122631-98-5) → C59H76N10O9 (170018-92-5)

Guidance literature:

Multi-step reaction with 9 steps

1: 79 percent / KF, celite / acetonitrile / 82 °C

2: NH₂NH₂ / methanol / 50 °C

3: NaBH₄, MgSO₄ / methanol

4: KF, celite / acetonitrile / 82 °C

5: NH₂NH₂ / methanol / 50 °C

6: 88 percent / CH₂Cl₂

7: TFA

8: TEA / CH₂Cl₂

9: TFA

With potassium fluoride; sodium tetrahydroborate; Celite; TEA; magnesium sulfate; trifluoroacetic acid; hydrazine; In methanol; dichloromethane; acetonitrile;

DOI:10.1016/S0040-4039(00)82310-2

Reference yield:

N4-benzyl-N9-(tert-butoxycarbonyl)-4-aza-1,9-diaminononane (170018-88-9) → C59H76N10O9 (170018-92-5)

Guidance literature:

Multi-step reaction with 7 steps

1: NaBH₄, MgSO₄ / methanol

2: KF, celite / acetonitrile / 82 °C

3: NH₂NH₂ / methanol / 50 °C

4: 88 percent / CH₂Cl₂

5: TFA

6: TEA / CH₂Cl₂

7: TFA

With potassium fluoride; sodium tetrahydroborate; Celite; TEA; magnesium sulfate; trifluoroacetic acid; hydrazine; In methanol; dichloromethane; acetonitrile;

DOI:10.1016/S0040-4039(00)82310-2

upstream raw materials:

C₆₄H₈₄N₁₀O₁₁

5-tert-butoxycarbonylamino-1-aminopentane

N¹-benzyl-N⁵-(tert-butoxycarbonyl)-1,5-diaminopentane

N⁴-benzyl-N⁹-(tert-butoxycarbonyl)-4-aza-1,9-diaminononane

Downstream raw materials:

Argiotoxin 659