C₄₁H₆₄O₆Si₃

Base Information

Chemical Name:C₄₁H₆₄O₆Si₃
CAS No.:945468-60-0
Molecular Formula:C₄₁H₆₄O₆Si₃
Molecular Weight:737.212
Hs Code.:

C<sub>41</sub>H<sub>64</sub>O<sub>6</sub>Si<sub>3</sub>

Synonyms:C₄₁H₆₄O₆Si₃

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Chemical Property of C₄₁H₆₄O₆Si₃

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Technology Process of C₄₁H₆₄O₆Si₃

There total 14 articles about C₄₁H₆₄O₆Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 945468-59-7
C₄₄H₇₀O₅S₂Si₃

: 945468-60-0
C₄₁H₆₄O₆Si₃

Guidance literature:: With 2,6-di-tert-butyl-pyridine; mercury(II) perchlorate; In tetrahydrofuran; water; at 25 ℃; for 0.25h;
DOI:10.1016/j.tetlet.2007.04.136

Reference yield:

: 945468-56-4
C₃₂H₄₂O₆Si

: 945468-60-0
C₄₁H₆₄O₆Si₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: 83 percent / NaH; Bu₄NI / tetrahydrofuran / 2 h / 23 °C

2.1: DDQ / CH₂Cl₂ / 3.5 h / 26 °C / pH 7

3.1: 2,6-lutidine / CH₂Cl₂ / 1 h / 0 °C

4.1: t-BuLi; Bu₂Mg / tetrahydrofuran / 0.5 h / -20 °C

4.2: 72 percent / tetrahydrofuran / 1 h / 23 °C

5.1: 87 percent / 2,6-lutidine / dimethylformamide / 1.17 h / 0 °C

6.1: 72 percent / Hg(ClO₄)2; 2,6-di-tert-butylpyridine / tetrahydrofuran; H₂O / 0.25 h / 25 °C

With 2,6-dimethylpyridine; 2,6-di-tert-butyl-pyridine; mercury(II) perchlorate; dibutylmagnesium; tert.-butyl lithium; tetra-(n-butyl)ammonium iodide; sodium hydride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2007.04.136

Reference yield:

: 945468-57-5
C₄₀H₅₀O₇Si

: 945468-60-0
C₄₁H₆₄O₆Si₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: DDQ / CH₂Cl₂ / 3.5 h / 26 °C / pH 7

2.1: 2,6-lutidine / CH₂Cl₂ / 1 h / 0 °C

3.1: t-BuLi; Bu₂Mg / tetrahydrofuran / 0.5 h / -20 °C

3.2: 72 percent / tetrahydrofuran / 1 h / 23 °C

4.1: 87 percent / 2,6-lutidine / dimethylformamide / 1.17 h / 0 °C

5.1: 72 percent / Hg(ClO₄)2; 2,6-di-tert-butylpyridine / tetrahydrofuran; H₂O / 0.25 h / 25 °C

With 2,6-dimethylpyridine; 2,6-di-tert-butyl-pyridine; mercury(II) perchlorate; dibutylmagnesium; tert.-butyl lithium; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2007.04.136