dimethyl [(4-chloro-2-cyano-1-morpholino-3-phenyl-1-buten-1-yl)thio]propanedioate

Base Information

Chemical Name:dimethyl [(4-chloro-2-cyano-1-morpholino-3-phenyl-1-buten-1-yl)thio]propanedioate
CAS No.:440364-26-1
Molecular Formula:C₂₀H₂₃ClN₂O₅S
Molecular Weight:438.932
Hs Code.:

Synonyms:dimethyl [(4-chloro-2-cyano-1-morpholino-3-phenyl-1-buten-1-yl)thio]propanedioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethyl [(4-chloro-2-cyano-1-morpholino-3-phenyl-1-buten-1-yl)thio]propanedioate

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Technology Process of dimethyl [(4-chloro-2-cyano-1-morpholino-3-phenyl-1-buten-1-yl)thio]propanedioate

There total 3 articles about dimethyl [(4-chloro-2-cyano-1-morpholino-3-phenyl-1-buten-1-yl)thio]propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 857635-46-2,440364-12-5
3-cyano-4,5-dihydro-2-morpholino-4-phenylthiophenium-1-bis(methoxycarbonyl)methylide

: 440364-26-1
dimethyl [(4-chloro-2-cyano-1-morpholino-3-phenyl-1-buten-1-yl)thio]propanedioate

Guidance literature:: With thionyl chloride; In chloroform; for 5h; Heating;
DOI:10.1002/jhet.5570390131

Reference yield:

: 6773-29-1
dimethyl diazomalonate

: 440364-26-1
dimethyl [(4-chloro-2-cyano-1-morpholino-3-phenyl-1-buten-1-yl)thio]propanedioate

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / rhodium(II) acetate dimer / toluene / 2 h / Heating

2: 76 percent / thionyl chloride / CHCl₃ / 5 h / Heating

With dirhodium tetraacetate; thionyl chloride; In chloroform; toluene;
DOI:10.1002/jhet.5570390131

Reference yield:

: 154001-04-4
4,5-dihydro-2-morpholino-4-phenyl-3-thiophenecarbonitrile

: 440364-26-1
dimethyl [(4-chloro-2-cyano-1-morpholino-3-phenyl-1-buten-1-yl)thio]propanedioate

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / rhodium(II) acetate dimer / toluene / 2 h / Heating

2: 76 percent / thionyl chloride / CHCl₃ / 5 h / Heating

With dirhodium tetraacetate; thionyl chloride; In chloroform; toluene;
DOI:10.1002/jhet.5570390131