4-[4,5-dihydro-1-(4-nitrophenyl)-5-(phenylethynyl)-1H-1,2,3-triazol-5-yl]morpholine

Base Information

Chemical Name:4-[4,5-dihydro-1-(4-nitrophenyl)-5-(phenylethynyl)-1H-1,2,3-triazol-5-yl]morpholine
CAS No.:866783-73-5
Molecular Formula:C₂₀H₁₉N₅O₃
Molecular Weight:377.403
Hs Code.:

Synonyms:4-[4,5-dihydro-1-(4-nitrophenyl)-5-(phenylethynyl)-1H-1,2,3-triazol-5-yl]morpholine

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Chemical Property of 4-[4,5-dihydro-1-(4-nitrophenyl)-5-(phenylethynyl)-1H-1,2,3-triazol-5-yl]morpholine

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Technology Process of 4-[4,5-dihydro-1-(4-nitrophenyl)-5-(phenylethynyl)-1H-1,2,3-triazol-5-yl]morpholine

There total 1 articles about 4-[4,5-dihydro-1-(4-nitrophenyl)-5-(phenylethynyl)-1H-1,2,3-triazol-5-yl]morpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1516-60-5
4-nitrophenyl azide

: 158586-36-8
4-(1-methylene-3-phenylprop-2-ynyl)morpholine

: 866783-73-5
4-[4,5-dihydro-1-(4-nitrophenyl)-5-(phenylethynyl)-1H-1,2,3-triazol-5-yl]morpholine

Guidance literature:: In toluene; at 22 ℃; for 10h; under 5437940 Torr;
DOI:10.1002/hlca.200590142

Reference yield: 58.0%

: 866783-73-5
4-[4,5-dihydro-1-(4-nitrophenyl)-5-(phenylethynyl)-1H-1,2,3-triazol-5-yl]morpholine

: 1-(4-nitrophenyl)-5-(phenylethynyl)-1H-1,2,3-triazole

Guidance literature:: In water; acetic acid; for 0.166667h; Heating;
DOI:10.1002/hlca.200590142

Reference yield:

: 866783-73-5
4-[4,5-dihydro-1-(4-nitrophenyl)-5-(phenylethynyl)-1H-1,2,3-triazol-5-yl]morpholine

: 1-(4-nitrophenyl)-5-[(1E)-2-phenoxy-2-phenylethenyl]-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 4 h / Heating

2: 76 mg / acetic acid; H₂O / 0.17 h / Heating

In water; acetic acid; toluene;
DOI:10.1002/hlca.200590142