(N-phenyltrifluoroacetimidoyl) 2-O-acetyl-3,7-di-O-benzoyl-4-O-para-bromobenzyl-6-O-benzyl-L-glycero-D-manno-heptopyranoside

Base Information

Chemical Name:(N-phenyltrifluoroacetimidoyl) 2-O-acetyl-3,7-di-O-benzoyl-4-O-para-bromobenzyl-6-O-benzyl-L-glycero-D-manno-heptopyranoside
CAS No.:1427441-91-5
Molecular Formula:C₄₅H₃₉BrF₃NO₁₀
Molecular Weight:890.705
Hs Code.:

Synonyms:(N-phenyltrifluoroacetimidoyl) 2-O-acetyl-3,7-di-O-benzoyl-4-O-para-bromobenzyl-6-O-benzyl-L-glycero-D-manno-heptopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (N-phenyltrifluoroacetimidoyl) 2-O-acetyl-3,7-di-O-benzoyl-4-O-para-bromobenzyl-6-O-benzyl-L-glycero-D-manno-heptopyranoside

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Technology Process of (N-phenyltrifluoroacetimidoyl) 2-O-acetyl-3,7-di-O-benzoyl-4-O-para-bromobenzyl-6-O-benzyl-L-glycero-D-manno-heptopyranoside

There total 1 articles about (N-phenyltrifluoroacetimidoyl) 2-O-acetyl-3,7-di-O-benzoyl-4-O-para-bromobenzyl-6-O-benzyl-L-glycero-D-manno-heptopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: C₃₇H₃₅BrO₁₀

: 61881-19-4
2,2,2-trifluoro-N-phenyl-acetimidoyl chloride

: 1427441-91-5
(N-phenyltrifluoroacetimidoyl) 2-O-acetyl-3,7-di-O-benzoyl-4-O-para-bromobenzyl-6-O-benzyl-L-glycero-D-manno-heptopyranoside

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ja401164s

Reference yield: 81.0%

: methyl 2,7-di-O-acetyl-4-O-para-bromobenzyl-6-O-benzyl-L-glycero-α-D-manno-heptopyranosyl-(1→5)-[4-azido-2,3-di-O-benzyl-4-deoxy-α-L-arabinopyranosyl-(1→8)]-(5-(N-benzyl-benzyloxycarbonylamino)pentyl 4-Obenzyl-7-O-acetyl-3-deoxy-α-D-manno-oct-2-ulopyranoside)onate

: 1427441-91-5
(N-phenyltrifluoroacetimidoyl) 2-O-acetyl-3,7-di-O-benzoyl-4-O-para-bromobenzyl-6-O-benzyl-L-glycero-D-manno-heptopyranoside

: methyl 2-O-acetyl-3,7-di-O-benzoyl-4-O-para-bromobenzyl-6-O-benzyl-L-glycero-α-D-manno-heptopyranosyl-(1→3)-2,7-di-O-acetyl-4-O-para-bromobenzyl-6-O-benzyl-L-glycero-α-D-manno-heptopyranosyl-(1→5)-[4-azido-2,3-di-O-benzyl-4-deoxy-α-L-arabinopyranosyl-(1→8)]-(5-(N-benzyl-benzyloxycarbonylamino)pentyl 4-O-benzyl-7-O-acetyl-3-deoxy-α-D-manno-oct-2-ulopyranoside)onate

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 - 20 ℃; for 1h; Inert atmosphere; Molecular sieve;
DOI:10.1021/ja401164s

Reference yield: 73.0%

: 1403362-18-4
methyl [N-benzyl-benzyloxycarbonyl-5-aminopentyl (2,7-di-O-acetyl-4-O-para-bromobenzyl-6-O-benzyl-L-glycero-α-D-manno-heptopyranosyl)-(1→5)-4-O-benzyl-7,8-O-isopropylidene-3-deoxy-α-D-manno-oct-2-ulopyranosid]onate

: 1427441-91-5
(N-phenyltrifluoroacetimidoyl) 2-O-acetyl-3,7-di-O-benzoyl-4-O-para-bromobenzyl-6-O-benzyl-L-glycero-D-manno-heptopyranoside

: 1429492-47-6
methyl [5-(N-benzyl-benzyloxycarbonylamino)pentyl (2-O-acetyl-3,7-di-O-benzoyl-4-O-para-bromobenzyl-6-O-benzyl-L-glycero-α-D-mannoheptopyranosyl)-(1→3)-(2,7-di-O-acetyl-4-O-para-bromobenzyl-6-O-benzyl-L-glycero-α-D-manno-heptopyranosyl)-(1→5)-4-O-benzyl-7,8-O-isopropylidene-3-deoxy-α-D-manno-oct-2-ulopyranosid]onate

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 - 20 ℃; for 1h; Inert atmosphere; Molecular sieve;
DOI:10.1021/ja401164s