2,6-bis<1-ethyl-5-(4-dodecyloxybenzoic ester)benzimidazol-2-yl>pyridine

Base Information

Chemical Name:2,6-bis<1-ethyl-5-(4-dodecyloxybenzoic ester)benzimidazol-2-yl>pyridine
CAS No.:200354-20-7
Molecular Formula:C₆₁H₇₇N₅O₆
Molecular Weight:976.312
Hs Code.:

Synonyms:2,6-bis<1-ethyl-5-(4-dodecyloxybenzoic ester)benzimidazol-2-yl>pyridine

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Chemical Property of 2,6-bis<1-ethyl-5-(4-dodecyloxybenzoic ester)benzimidazol-2-yl>pyridine

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Technology Process of 2,6-bis<1-ethyl-5-(4-dodecyloxybenzoic ester)benzimidazol-2-yl>pyridine

There total 8 articles about 2,6-bis<1-ethyl-5-(4-dodecyloxybenzoic ester)benzimidazol-2-yl>pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3739-94-4
2,6-Pyridinedicarbonyl dichloride

: 200354-20-7
2,6-bis<1-ethyl-5-(4-dodecyloxybenzoic ester)benzimidazol-2-yl>pyridine

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / Et₃N / CH₂Cl₂ / 8 h / Heating

2: 60 percent / Fe, aq. HCl / ethanol / 12 h / Heating

3: 1.) BBr₃, 2.) aq. NaHCO₃ / 1.) CH₂Cl₂, RT, 3 h, 2.) CH₂Cl₂

4: 1.) NBu₄OH / 1.) CH₂Cl₂, MeOH, 2.) CH₂Cl₂, 10 h

With hydrogenchloride; tetra(n-butyl)ammonium hydroxide; boron tribromide; iron; sodium hydrogencarbonate; triethylamine; In ethanol; dichloromethane;
DOI:10.1021/ja982545n

Reference yield:

: 10298-80-3
2-chloro-5-methoxynitrobenzene

: 200354-20-7
2,6-bis<1-ethyl-5-(4-dodecyloxybenzoic ester)benzimidazol-2-yl>pyridine

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / H₂O / 12 h / 100 °C

2: 75 percent / Et₃N / CH₂Cl₂ / 8 h / Heating

3: 60 percent / Fe, aq. HCl / ethanol / 12 h / Heating

4: 1.) BBr₃, 2.) aq. NaHCO₃ / 1.) CH₂Cl₂, RT, 3 h, 2.) CH₂Cl₂

5: 1.) NBu₄OH / 1.) CH₂Cl₂, MeOH, 2.) CH₂Cl₂, 10 h

With hydrogenchloride; tetra(n-butyl)ammonium hydroxide; boron tribromide; iron; sodium hydrogencarbonate; triethylamine; In ethanol; dichloromethane; water;
DOI:10.1021/ja982545n

Reference yield:

: 218143-47-6
bispyridine-2,6-dicarboxamide

: 200354-20-7
2,6-bis<1-ethyl-5-(4-dodecyloxybenzoic ester)benzimidazol-2-yl>pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / Fe, aq. HCl / ethanol / 12 h / Heating

2: 1.) BBr₃, 2.) aq. NaHCO₃ / 1.) CH₂Cl₂, RT, 3 h, 2.) CH₂Cl₂

3: 1.) NBu₄OH / 1.) CH₂Cl₂, MeOH, 2.) CH₂Cl₂, 10 h

With hydrogenchloride; tetra(n-butyl)ammonium hydroxide; boron tribromide; iron; sodium hydrogencarbonate; In ethanol;
DOI:10.1021/ja982545n