Technology Process of C64H84N4O12S2
There total 8 articles about C64H84N4O12S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine;
In
dichloromethane;
at 0 - 20 ℃;
for 18h;
Inert atmosphere;
DOI:10.1002/chem.201204556
- Guidance literature:
-
Multi-step reaction with 7 steps
1: potassium carbonate / methanol / 2 h / 0 - 20 °C / Inert atmosphere
2: triethylamine / dichloromethane / 3 h / -100 - 0 °C / Inert atmosphere
3: 1,1'-bis-(diphenylphosphino)ferrocene; sodium t-butanolate; palladium diacetate / toluene / 1 h / 100 °C / Inert atmosphere
4: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere
5: potassium hydroxide; oxygen / N,N-dimethyl-formamide / 120 h / 70 °C
6: thionyl chloride; N,N-dimethyl-formamide / 6 h / 60 °C / Inert atmosphere
7: pyridine / dichloromethane / 18 h / 0 - 20 °C / Inert atmosphere
With
pyridine; 1,1'-bis-(diphenylphosphino)ferrocene; thionyl chloride; tetrabutyl ammonium fluoride; oxygen; palladium diacetate; potassium carbonate; acetic acid; triethylamine; N,N-dimethyl-formamide; potassium hydroxide; sodium t-butanolate;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/chem.201204556
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium hydroxide; oxygen / N,N-dimethyl-formamide / 120 h / 70 °C
2: thionyl chloride; N,N-dimethyl-formamide / 6 h / 60 °C / Inert atmosphere
3: pyridine / dichloromethane / 18 h / 0 - 20 °C / Inert atmosphere
With
pyridine; thionyl chloride; oxygen; N,N-dimethyl-formamide; potassium hydroxide;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201204556