1-Pyridin-2-yl-2-(2-pyrrol-1-yl-benzylsulfanyl)-1,4,5,6-tetrahydro-cyclopentaimidazole

Base Information

Chemical Name:1-Pyridin-2-yl-2-(2-pyrrol-1-yl-benzylsulfanyl)-1,4,5,6-tetrahydro-cyclopentaimidazole
CAS No.:117323-80-5
Molecular Formula:C₂₂H₂₀N₄S
Molecular Weight:372.494
Hs Code.:

Synonyms:1-Pyridin-2-yl-2-(2-pyrrol-1-yl-benzylsulfanyl)-1,4,5,6-tetrahydro-cyclopentaimidazole

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Chemical Property of 1-Pyridin-2-yl-2-(2-pyrrol-1-yl-benzylsulfanyl)-1,4,5,6-tetrahydro-cyclopentaimidazole

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Technology Process of 1-Pyridin-2-yl-2-(2-pyrrol-1-yl-benzylsulfanyl)-1,4,5,6-tetrahydro-cyclopentaimidazole

There total 5 articles about 1-Pyridin-2-yl-2-(2-pyrrol-1-yl-benzylsulfanyl)-1,4,5,6-tetrahydro-cyclopentaimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 101130-77-2
1-(2-(chloromethyl)phenyl)-1H-pyrrole

: 1-Pyridin-2-yl-3,4,5,6-tetrahydro-1H-cyclopentaimidazole-2-thione

: 117323-80-5
1-Pyridin-2-yl-2-(2-pyrrol-1-yl-benzylsulfanyl)-1,4,5,6-tetrahydro-cyclopentaimidazole

Guidance literature:: With sodium hydroxide; In N,N-dimethyl-formamide; at 0 ℃; for 3h;
DOI:10.1021/jm950610n

Reference yield:

: 10333-67-2
methyl 2-(1H-pyrrol-1-yl)benzoate

: 117323-80-5
1-Pyridin-2-yl-2-(2-pyrrol-1-yl-benzylsulfanyl)-1,4,5,6-tetrahydro-cyclopentaimidazole

Guidance literature:: Multi-step reaction with 3 steps

1: LiAlH₄ / tetrahydrofuran

2: SOCl₂ / CHCl₃

3: NaOH / dimethylformamide / 3 h / 0 °C

With sodium hydroxide; lithium aluminium tetrahydride; thionyl chloride; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jm950610n

Reference yield:

: 61034-86-4
2-(pyrrol-1-yl)-benzyl alcohol

: 117323-80-5
1-Pyridin-2-yl-2-(2-pyrrol-1-yl-benzylsulfanyl)-1,4,5,6-tetrahydro-cyclopentaimidazole

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / CHCl₃

2: NaOH / dimethylformamide / 3 h / 0 °C

With sodium hydroxide; thionyl chloride; In chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jm950610n