S,S,S-2-azabicyclo[3,3,0]-octane-3-carboxylic acid benzyl ester L-mandelic acid salt

Base Information

Chemical Name:S,S,S-2-azabicyclo[3,3,0]-octane-3-carboxylic acid benzyl ester L-mandelic acid salt
CAS No.:135214-79-8
Molecular Formula:C₈H₈O₃*C₁₅H₁₉NO₂
Molecular Weight:397.471
Hs Code.:

Synonyms:S,S,S-2-azabicyclo[3,3,0]-octane-3-carboxylic acid benzyl ester L-mandelic acid salt

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Chemical Property of S,S,S-2-azabicyclo[3,3,0]-octane-3-carboxylic acid benzyl ester L-mandelic acid salt

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Technology Process of S,S,S-2-azabicyclo[3,3,0]-octane-3-carboxylic acid benzyl ester L-mandelic acid salt

There total 2 articles about S,S,S-2-azabicyclo[3,3,0]-octane-3-carboxylic acid benzyl ester L-mandelic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17199-29-0
(S)-Mandelic acid

: 87269-87-2,87679-25-2,88547-79-9,93779-29-4,94569-19-4,138877-09-5
(1RS,3RS,5RS)-2-Azabicyclo<3.3.0>octan-3-carbonsaeurebenzylester-hydrochlorid

: 135214-79-8
S,S,S-2-azabicyclo[3,3,0]-octane-3-carboxylic acid benzyl ester L-mandelic acid salt

: (R,R,R)-2-azabicyclo[3.3.0]octane-3-carboxylic acid benzyl ester mandelic acid salt

Guidance literature:: (1RS,3RS,5RS)-2-Azabicyclo<3.3.0>octan-3-carbonsaeurebenzylester-hydrochlorid; With sodium hydroxide; In water; ethyl acetate; Resolution of racemate;

(S)-Mandelic acid; In ethyl acetate;

Reference yield:

: 951665-42-2
(1S,5S)-2-azabicyclo[3,3,0]-octane-3-carboxylic acid benzyl ester

: 17199-29-0
(S)-Mandelic acid

: 135214-79-8
S,S,S-2-azabicyclo[3,3,0]-octane-3-carboxylic acid benzyl ester L-mandelic acid salt

Guidance literature:: In ethyl acetate; at 22 - 28 ℃; for 0.166667 - 0.25h; Product distribution / selectivity;

Reference yield: 91.0%

: 135214-79-8
S,S,S-2-azabicyclo[3,3,0]-octane-3-carboxylic acid benzyl ester L-mandelic acid salt

: 87269-87-2,87679-25-2,88547-79-9,93779-29-4,94569-19-4,138877-09-5
benzyl (2S,3AS,6AS)-octahydrocyclopenta[b]pyrrole-2-carboxylate hydrochloride

Guidance literature:: S,S,S-2-azabicyclo[3,3,0]-octane-3-carboxylic acid benzyl ester L-mandelic acid salt; With sodium hydroxide; In dichloromethane; water; at 25 - 30 ℃;

With hydrogenchloride; In water; isopropyl alcohol;