Technology Process of C36H41F2N5O5Si
There total 5 articles about C36H41F2N5O5Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C
2.1: ammonium sulfate / 18 h / Inert atmosphere
2.2: Reflux
3.1: silver nitrate; 2,4,6-trimethyl-pyridine / dichloromethane / 12 h / 0 - 20 °C
4.1: sodium methylate; 2-hydroxyethanethiol / methanol / Reflux
5.1: pyridine; 4,4'-dimethoxytrityl chloride / 15 h / 0 - 20 °C
5.2: 12 h / 20 °C
5.3: 3 h / -78 - -20 °C
With
pyridine; 2,4,6-trimethyl-pyridine; ammonium sulfate; 4,4'-dimethoxytrityl chloride; sodium methylate; silver nitrate; triethylamine; 2-hydroxyethanethiol;
In
methanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium methylate; 2-hydroxyethanethiol / methanol / Reflux
2.1: pyridine; 4,4'-dimethoxytrityl chloride / 15 h / 0 - 20 °C
2.2: 12 h / 20 °C
2.3: 3 h / -78 - -20 °C
With
pyridine; 4,4'-dimethoxytrityl chloride; sodium methylate; 2-hydroxyethanethiol;
In
methanol;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: lithium tri-t-butoxyaluminum hydride / tetrahydrofuran / 2 h / -78 - 20 °C / Inert atmosphere
2.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C
3.1: ammonium sulfate / 18 h / Inert atmosphere
3.2: Reflux
4.1: silver nitrate; 2,4,6-trimethyl-pyridine / dichloromethane / 12 h / 0 - 20 °C
5.1: sodium methylate; 2-hydroxyethanethiol / methanol / Reflux
6.1: pyridine; 4,4'-dimethoxytrityl chloride / 15 h / 0 - 20 °C
6.2: 12 h / 20 °C
6.3: 3 h / -78 - -20 °C
With
pyridine; 2,4,6-trimethyl-pyridine; ammonium sulfate; 4,4'-dimethoxytrityl chloride; sodium methylate; silver nitrate; lithium tri-t-butoxyaluminum hydride; triethylamine; 2-hydroxyethanethiol;
In
tetrahydrofuran; methanol; dichloromethane;