1-(3,3-dimethyl-2-phenylcyclopent-1-en-1-yl)-4-(trifluoromethoxy)benzene

Base Information

Chemical Name:1-(3,3-dimethyl-2-phenylcyclopent-1-en-1-yl)-4-(trifluoromethoxy)benzene
CAS No.:1618681-48-3
Molecular Formula:C₂₀H₁₉F₃O
Molecular Weight:332.365
Hs Code.:

Synonyms:1-(3,3-dimethyl-2-phenylcyclopent-1-en-1-yl)-4-(trifluoromethoxy)benzene

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Chemical Property of 1-(3,3-dimethyl-2-phenylcyclopent-1-en-1-yl)-4-(trifluoromethoxy)benzene

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Technology Process of 1-(3,3-dimethyl-2-phenylcyclopent-1-en-1-yl)-4-(trifluoromethoxy)benzene

There total 2 articles about 1-(3,3-dimethyl-2-phenylcyclopent-1-en-1-yl)-4-(trifluoromethoxy)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 62707-15-7
(5-methylhex-1-yn-1-yl)benzene

: 1618681-41-6
C₁₆H₁₅F₃IO⁽¹⁺⁾*F₆P^(1-)

: 1618681-48-3
1-(3,3-dimethyl-2-phenylcyclopent-1-en-1-yl)-4-(trifluoromethoxy)benzene

Guidance literature:: C₁₆H₁₅F₃IO⁽¹⁺⁾*F₆P^(1-); With copper(II) bis(trifluoromethanesulfonate); at 80 ℃; for 1h; Inert atmosphere; Sealed tube; Schlenk technique;

(5-methylhex-1-yn-1-yl)benzene; In 1,2-dichloro-ethane; at 60 ℃; for 12h; Inert atmosphere; Sealed tube; Schlenk technique;
DOI:10.1021/ol501655g

Reference yield:

: mesityl[4-(trifluoromethoxy)phenyl]iodonium trifluoromethanesulfonate

: 1618681-48-3
1-(3,3-dimethyl-2-phenylcyclopent-1-en-1-yl)-4-(trifluoromethoxy)benzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hexafluorophosphate / acetonitrile / 24 h / Inert atmosphere; Sealed tube

2.1: copper(II) bis(trifluoromethanesulfonate) / 1 h / 80 °C / Inert atmosphere; Sealed tube; Schlenk technique

2.2: 12 h / 60 °C / Inert atmosphere; Sealed tube; Schlenk technique

With potassium hexafluorophosphate; copper(II) bis(trifluoromethanesulfonate); In acetonitrile;
DOI:10.1021/ol501655g