C₂₀H₂₀SO₆

Base Information

Chemical Name:C₂₀H₂₀SO₆
CAS No.:937164-03-9
Molecular Formula:C₂₀H₂₀O₆S
Molecular Weight:388.441
Hs Code.:

C<sub>20</sub>H<sub>20</sub>SO<sub>6</sub>

Synonyms:C₂₀H₂₀SO₆

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Chemical Property of C₂₀H₂₀SO₆

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Technology Process of C₂₀H₂₀SO₆

There total 1 articles about C₂₀H₂₀SO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 98-59-9
p-toluenesulfonyl chloride

: 279684-68-3
(2R,3R,4S)-hex-5-yn-2,3,4-triol 2-benzoate ester

: 937164-03-9
C₂₀H₂₀SO₆

Guidance literature:: (2R,3R,4S)-hex-5-yn-2,3,4-triol 2-benzoate ester; With di(n-butyl)tin oxide; In toluene; at 110 ℃; for 5h;

p-toluenesulfonyl chloride; In toluene; at 20 ℃; for 24h; Further stages.;
DOI:10.1021/ol070435s

Reference yield: 75.0%

: 937164-03-9
C₂₀H₂₀SO₆

: 937164-04-0
C₁₃H₁₃N₃O₃

Guidance literature:: With sodium azide; 15-crown-5; In dimethyl sulfoxide; at 20 ℃;
DOI:10.1021/ol070435s

Reference yield:

: 937164-03-9
C₂₀H₂₀SO₆

: C₁₆H₂₁NO₅

Guidance literature:: Multi-step reaction with 5 steps

1: 75 percent / NaN₃; 15-crown-5 / dimethylsulfoxide / 20 °C

2: 71 percent / P₂O₅ / 0.5 h / 20 °C

3: lithium aluminum hydride / tetrahydrofuran / 3 h / 0 °C

4: 0.120 g / K₂CO₃ / acetone; H₂O / 0.17 h / 20 °C

5: 95 percent / triethylamine / (methoxymethylcarbene)pentacarbonyl tungsten / tetrahydrofuran / 12 h / 40 °C

With lithium aluminium tetrahydride; sodium azide; 15-crown-5; phosphorus pentoxide; potassium carbonate; triethylamine; (methoxymethylcarbene)pentacarbonyl tungsten; In tetrahydrofuran; water; dimethyl sulfoxide; acetone;
DOI:10.1021/ol070435s