N-α-(9-fluorenylmethyloxycarbonyl)-O--L-phosphotyrosine

Base Information

Chemical Name:N-α-(9-fluorenylmethyloxycarbonyl)-O--L-phosphotyrosine
CAS No.:217792-95-5
Molecular Formula:C₃₈H₄₆NO₁₀PS₂
Molecular Weight:771.89
Hs Code.:

N-α-(9-fluorenylmethyloxycarbonyl)-O-<bis(S-pivaloyl-2-thioethyl)>-L-phosphotyrosine

Synonyms:N-α-(9-fluorenylmethyloxycarbonyl)-O--L-phosphotyrosine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-α-(9-fluorenylmethyloxycarbonyl)-O--L-phosphotyrosine

Chemical Property:

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Technology Process of N-α-(9-fluorenylmethyloxycarbonyl)-O--L-phosphotyrosine

There total 1 articles about N-α-(9-fluorenylmethyloxycarbonyl)-O--L-phosphotyrosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 112883-29-1,92954-90-0
N-Fmoc-Tyr-OH

: bis(S-pivaloyl-2-thioethyl)-N,N-diisopropylphosphoramidite

: 217792-95-5
N-α-(9-fluorenylmethyloxycarbonyl)-O--L-phosphotyrosine

Guidance literature:: Yield given; Multistep reaction;
DOI:10.1021/jo980437d

Reference yield: 80.0%

: 217792-95-5
N-α-(9-fluorenylmethyloxycarbonyl)-O--L-phosphotyrosine

: O--L-phosphotyrosine

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; for 0.166667h;
DOI:10.1021/jo980437d

Reference yield:

: 217792-95-5
N-α-(9-fluorenylmethyloxycarbonyl)-O--L-phosphotyrosine

: 217792-91-1
2,2-dimethyl-thiopropionic acid S-(2-{[4-(2-amino-2-{[({[1-(1-carbamoyl-3-methyl-butylcarbamoyl)-2-phenyl-ethylcarbamoyl]-methyl}-carbamoyl)-methyl]-carbamoyl}-ethyl)-phenoxy]-[2-(2,2-dimethyl-propionylsulfanyl)-ethoxy]-phosphoryloxy}-ethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 300 mg / N,N-diisopropyl-N-ethylamine, benzotriazol-1-yloxy-tris(dimethylamino)phosphonium hexafluorophosphate / CH₂Cl₂ / 2 h / Ambient temperature

2: 82 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene / CH₂Cl₂ / 0.25 h

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jo980437d