C₄₆H₅₆NiO₁₀S₄

Base Information

• Chemical Name: C₄₆H₅₆NiO₁₀S₄
• CAS No.: 1310676-15-3
• Molecular Formula: C₄₆H₅₆NiO₁₀S₄
• Molecular Weight: 955.899
• Mol file: 1310676-15-3.mol

Synonyms:C₄₆H₅₆NiO₁₀S₄

Chemical Property of C₄₆H₅₆NiO₁₀S₄

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₄₆H₅₆NiO₁₀S₄

There total 2 articles about C₄₆H₅₆NiO₁₀S₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

C23H30O7 (1400991-97-0) → C46H56NiO10S4 (1310676-15-3)

Guidance literature:

C₂₃H₃₀O₇; With tetraphosphorus decasulfide; In 1,4-dioxane; at 60 ℃; for 2h;

With nickel(II) chloride hexahydrate; In 1,4-dioxane; at 110 ℃; for 3h;

DOI:10.1080/15421406.2012.691676

Reference yield:

3,4-dihydroxybenzaldehyde (139-85-5) → C46H56NiO10S4 (1310676-15-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium carbonate; potassium iodide / N,N-dimethyl-formamide / 4 h / 13 °C

2.1: potassium cyanide / ethanol; water / 4 h / 20 °C

3.1: tetraphosphorus decasulfide / 1,4-dioxane / 2 h / 60 °C

3.2: 3 h / 110 °C

With potassium cyanide; tetraphosphorus decasulfide; sodium carbonate; potassium iodide; In 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide;

DOI:10.1080/15421406.2012.691676

upstream raw materials:

C₂₃H₃₀O₇

3,4-dihydroxybenzaldehyde