N-ethyl-N-[4-(4-nitrophenylazo)-phenyl]aminoethyl 3α,7α,12α-tris[(phenylaminocarbonyl)amino]-5β-cholan-24-oate

Base Information

Chemical Name:N-ethyl-N-[4-(4-nitrophenylazo)-phenyl]aminoethyl 3α,7α,12α-tris[(phenylaminocarbonyl)amino]-5β-cholan-24-oate
CAS No.:1352749-34-8
Molecular Formula:C₆₁H₇₄N₁₀O₇
Molecular Weight:1059.32
Hs Code.:

Synonyms:N-ethyl-N-[4-(4-nitrophenylazo)-phenyl]aminoethyl 3α,7α,12α-tris[(phenylaminocarbonyl)amino]-5β-cholan-24-oate

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Chemical Property of N-ethyl-N-[4-(4-nitrophenylazo)-phenyl]aminoethyl 3α,7α,12α-tris[(phenylaminocarbonyl)amino]-5β-cholan-24-oate

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Technology Process of N-ethyl-N-[4-(4-nitrophenylazo)-phenyl]aminoethyl 3α,7α,12α-tris[(phenylaminocarbonyl)amino]-5β-cholan-24-oate

There total 2 articles about N-ethyl-N-[4-(4-nitrophenylazo)-phenyl]aminoethyl 3α,7α,12α-tris[(phenylaminocarbonyl)amino]-5β-cholan-24-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1243065-14-6
3α,7α,12α-tris[(phenylaminocarbonyl)amino]-5β-cholic acid

: 98343-67-0
2-{ethyl[4-(4-nitrophenyldiazenyl)phenyl]amino}ethyl methanesulfonate

: 1352749-34-8
N-ethyl-N-[4-(4-nitrophenylazo)-phenyl]aminoethyl 3α,7α,12α-tris[(phenylaminocarbonyl)amino]-5β-cholan-24-oate

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1002/anie.201105216

Reference yield:

: methyl 3α,7α,12α-tris[(phenylaminocarbonyl)amino]-5β-cholan-24-oate

: 1352749-34-8
N-ethyl-N-[4-(4-nitrophenylazo)-phenyl]aminoethyl 3α,7α,12α-tris[(phenylaminocarbonyl)amino]-5β-cholan-24-oate

Guidance literature:: Multi-step reaction with 2 steps

1: water

2: caesium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

With water; caesium carbonate; In N,N-dimethyl-formamide;
DOI:10.1002/anie.201105216