C₃₄H₃₆N₂O₁₀

Base Information

• Chemical Name: C₃₄H₃₆N₂O₁₀
• CAS No.: 1280608-87-8
• Molecular Formula: C₃₄H₃₆N₂O₁₀
• Molecular Weight: 632.667
• Mol file: 1280608-87-8.mol

Synonyms:C₃₄H₃₆N₂O₁₀

Chemical Property of C₃₄H₃₆N₂O₁₀

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₄H₃₆N₂O₁₀

There total 11 articles about C₃₄H₃₆N₂O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

C39H50N2O11Si (1280608-67-4) → C34H36N2O10 (1280608-87-8)

Guidance literature:

With toluene-4-sulfonic acid; In tetrahydrofuran; water; for 4.5h; Reflux;

DOI:10.1002/anie.201006528

Reference yield:

C23H25NO6 (1280608-40-3) → C34H36N2O10 (1280608-87-8)

Guidance literature:

Multi-step reaction with 10 steps

1.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C

2.2: 2.5 h / 20 °C

3.1: Oxone; C₁₃H₂₀O₉; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / Dimethoxymethane; water; acetonitrile / 24 h / 0 °C / pH 6 / aq. phosphate buffer

4.1: water; pyridinium p-toluenesulfonate / 1,4-dioxane / 12 h / 70 °C

5.1: [bis(acetoxy)iodo]benzene; potassium hydroxide / 2 h / 0 °C

6.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

7.1: pyridine; pyridine hydrofluoride / tetrahydrofuran / 8 h / -78 - 0 °C

8.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0 - 20 °C

9.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

9.2: -78 °C / Inert atmosphere

10.1: toluene-4-sulfonic acid / tetrahydrofuran; water / 4.5 h / Reflux

With pyridine; 2,6-dimethylpyridine; Oxone; sodium tetrahydroborate; n-butyllithium; C₁₃H₂₀O₉; pyridine hydrofluoride; [bis(acetoxy)iodo]benzene; water; tetra(n-butyl)ammonium hydrogensulfate; pyridinium p-toluenesulfonate; sodium hydride; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; toluene-4-sulfonic acid; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; Dimethoxymethane; hexane; dichloromethane; water; acetonitrile; mineral oil; 3.1: Shi epoxidation / 8.1: Dess-Martin oxidation;

DOI:10.1002/anie.201006528

Reference yield:

C23H27NO6 (1280608-50-5) → C34H36N2O10 (1280608-87-8)

Guidance literature:

Multi-step reaction with 9 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C

1.2: 2.5 h / 20 °C

2.1: Oxone; C₁₃H₂₀O₉; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / Dimethoxymethane; water; acetonitrile / 24 h / 0 °C / pH 6 / aq. phosphate buffer

3.1: water; pyridinium p-toluenesulfonate / 1,4-dioxane / 12 h / 70 °C

4.1: [bis(acetoxy)iodo]benzene; potassium hydroxide / 2 h / 0 °C

5.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

6.1: pyridine; pyridine hydrofluoride / tetrahydrofuran / 8 h / -78 - 0 °C

7.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0 - 20 °C

8.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

8.2: -78 °C / Inert atmosphere

9.1: toluene-4-sulfonic acid / tetrahydrofuran; water / 4.5 h / Reflux

With pyridine; 2,6-dimethylpyridine; Oxone; n-butyllithium; C₁₃H₂₀O₉; pyridine hydrofluoride; [bis(acetoxy)iodo]benzene; water; tetra(n-butyl)ammonium hydrogensulfate; pyridinium p-toluenesulfonate; sodium hydride; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; toluene-4-sulfonic acid; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; Dimethoxymethane; hexane; dichloromethane; water; acetonitrile; mineral oil; 2.1: Shi epoxidation / 7.1: Dess-Martin oxidation;

DOI:10.1002/anie.201006528

upstream raw materials:

C₂₁H₂₁NO₆

C₂₃H₂₅NO₆

C₂₃H₂₇NO₆

C₃₀H₃₃NO₆

Downstream raw materials:

C₃₄H₃₄N₂O₁₀

Refernces