methylphenylvinylphosphane borane

Base Information

• Chemical Name: methylphenylvinylphosphane borane
• CAS No.: 1020416-85-6
• Molecular Formula: C₉H₁₄BP
• Molecular Weight: 163.995
• Mol file: 1020416-85-6.mol

Synonyms:methylphenylvinylphosphane borane

Chemical Property of methylphenylvinylphosphane borane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methylphenylvinylphosphane borane

There total 1 articles about methylphenylvinylphosphane borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

2-(boranatomethylphenyl)phosphanylethyl methanesulfonate (485845-79-2) → methylphenylvinylphosphane borane (1020416-85-6)

Guidance literature:

With potassium tert-butoxide; In toluene; (Ar, Schlenk) potassium tert-butoxide was added as powder to sulfonate-compound in toluene, the mixt. was stirred for 1 h at 25°C; H2O was added, the organic layer was sepd., the aq. layer was extd. withethyl acetate, washed with aq. NaHCO3 and brine, dried with MgSO4, the solvent was removed at reduced pressure, flash chromy. on silica gel (et hyl acetate); as an oil;

DOI:10.1021/om701242t

upstream raw materials:

2-(boranatomethylphenyl)phosphanylethyl methanesulfonate