BOH(CH₃)2NCH₂C₆H₄⁽¹⁺⁾*B(C₆F₅)4^(1-)=BOH(CH₃)2NCH₂C₆H₄B(C₆F₅)4

Base Information

• Chemical Name: BOH(CH₃)2NCH₂C₆H₄⁽¹⁺⁾*B(C₆F₅)4^(1-)=BOH(CH₃)2NCH₂C₆H₄B(C₆F₅)4
• CAS No.: 1192230-03-7
• Molecular Formula: C₉H₁₃BNO*C₂₄BF₂₀
• Molecular Weight: 841.062

Synonyms:BOH(CH₃)2NCH₂C₆H₄⁽¹⁺⁾*B(C₆F₅)4^(1-)=BOH(CH₃)2NCH₂C₆H₄B(C₆F₅)4

Chemical Property of BOH(CH₃)2NCH₂C₆H₄⁽¹⁺⁾*B(C₆F₅)4^(1-)=BOH(CH₃)2NCH₂C₆H₄B(C₆F₅)4

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Technology Process of BOH(CH₃)2NCH₂C₆H₄⁽¹⁺⁾*B(C₆F₅)4^(1-)=BOH(CH₃)2NCH₂C₆H₄B(C₆F₅)4

There total 6 articles about BOH(CH₃)2NCH₂C₆H₄⁽¹⁺⁾*B(C₆F₅)4^(1-)=BOH(CH₃)2NCH₂C₆H₄B(C₆F₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

BH2(CH3)2NCH2C6H4 (185825-70-1) + trityl tetrakis(pentafluorophenyl)borate → BOH(CH3)2NCH2C6H4(1+)*B(C6F5)4(1-)=BOH(CH3)2NCH2C6H4B(C6F5)4 (1192230-03-7)

Guidance literature:

BH₂(CH₃)2NCH₂C₆H₄; trityl tetrakis(pentafluorophenyl)borate; In benzene; at 20 ℃; for 0.166667h; Inert atmosphere;

With water; In benzene; at 20 ℃; for 0.166667h; Inert atmosphere;

DOI:10.1021/ja905369n

Reference yield:

(CH3)3CC6H4CH2N(CH3)2 → BOH(CH3)2NCH2C6H4(1+)*B(C6F5)4(1-)=BOH(CH3)2NCH2C6H4B(C6F5)4 (1192230-03-7)

Guidance literature:

Multi-step reaction with 3 steps

1: not given

2: trityl tetrakis(pentafluorophenyl)borate / further solvent(s)

3: dichloromethane-d2

With trityl tetrakis(pentafluorophenyl)borate; In dichloromethane-d2;

DOI:10.1021/ja905369n

Reference yield:

2-(N,N-dimethylaminomethyl)phenyllithium (56174-66-4) → BOH(CH3)2NCH2C6H4(1+)*B(C6F5)4(1-)=BOH(CH3)2NCH2C6H4B(C6F5)4 (1192230-03-7)

Guidance literature:

Multi-step reaction with 3 steps

1: not given

2: not given

3: dichloromethane-d2

In dichloromethane-d2;

DOI:10.1021/ja905369n

upstream raw materials:

BH₂(CH₃)2NCH₂C₆H₄

water

2-(N,N-dimethylaminomethyl)phenyllithium

(CH₃)3SiC₆H₄CH₂N(CH₃)2BH₃

Downstream raw materials:

C₉H₁₄BNO₂*C₂₄BF₂₀^(1-)*H⁽¹⁺⁾

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