(R)-methyl (6-(4-nitrophenylsulfonamido)-1-phenylhex-1-yn-3-yl)carbonate

Base Information

Chemical Name:(R)-methyl (6-(4-nitrophenylsulfonamido)-1-phenylhex-1-yn-3-yl)carbonate
CAS No.:1580522-28-6
Molecular Formula:C₂₀H₂₀N₂O₇S
Molecular Weight:432.454
Hs Code.:

Synonyms:(R)-methyl (6-(4-nitrophenylsulfonamido)-1-phenylhex-1-yn-3-yl)carbonate

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Chemical Property of (R)-methyl (6-(4-nitrophenylsulfonamido)-1-phenylhex-1-yn-3-yl)carbonate

Chemical Property:

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Technology Process of (R)-methyl (6-(4-nitrophenylsulfonamido)-1-phenylhex-1-yn-3-yl)carbonate

There total 3 articles about (R)-methyl (6-(4-nitrophenylsulfonamido)-1-phenylhex-1-yn-3-yl)carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1353021-67-6
(R)-6-hydroxy-1-phenylhex-1-yn-3-yl methyl carbonate

: 1580522-28-6
(R)-methyl (6-(4-nitrophenylsulfonamido)-1-phenylhex-1-yn-3-yl)carbonate

Guidance literature:: Multi-step reaction with 3 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C / Inert atmosphere

2: potassium carbonate / methanol / 70 °C / Inert atmosphere

3: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

With pyridine; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/anie.201309162

Reference yield:

: 895153-23-8
N-(tert-butoxycarbonyl)-4-nitrobenzenesulfonamide

: 1580522-28-6
(R)-methyl (6-(4-nitrophenylsulfonamido)-1-phenylhex-1-yn-3-yl)carbonate

Guidance literature:: Multi-step reaction with 3 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C / Inert atmosphere

2: potassium carbonate / methanol / 70 °C / Inert atmosphere

3: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

With pyridine; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/anie.201309162

Reference yield:

: C₂₅H₂₈N₂O₉S

: 1580522-28-6
(R)-methyl (6-(4-nitrophenylsulfonamido)-1-phenylhex-1-yn-3-yl)carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / methanol / 70 °C / Inert atmosphere

2: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

With pyridine; potassium carbonate; In methanol; dichloromethane;
DOI:10.1002/anie.201309162