methyl (3,4-di-O-benzyl-α-L-idopyranosyluronic acid)-(1->4)-[2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl]-(1->4)-(3-O-benzyl-α-L-idopyranosideuronic acid)

Base Information

Chemical Name:methyl (3,4-di-O-benzyl-α-L-idopyranosyluronic acid)-(1->4)-[2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl]-(1->4)-(3-O-benzyl-α-L-idopyranosideuronic acid)
CAS No.:1075217-52-5
Molecular Formula:C₄₇H₅₃N₃O₁₇
Molecular Weight:931.948
Hs Code.:

methyl (3,4-di-O-benzyl-α-L-idopyranosyluronic acid)-(1->4)-[2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl]-(1->4)-(3-O-benzyl-α-L-idopyranosideuronic acid)

Synonyms:methyl (3,4-di-O-benzyl-α-L-idopyranosyluronic acid)-(1->4)-[2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl]-(1->4)-(3-O-benzyl-α-L-idopyranosideuronic acid)

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Chemical Property of methyl (3,4-di-O-benzyl-α-L-idopyranosyluronic acid)-(1->4)-[2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl]-(1->4)-(3-O-benzyl-α-L-idopyranosideuronic acid)

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Technology Process of methyl (3,4-di-O-benzyl-α-L-idopyranosyluronic acid)-(1->4)-[2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl]-(1->4)-(3-O-benzyl-α-L-idopyranosideuronic acid)

There total 1 articles about methyl (3,4-di-O-benzyl-α-L-idopyranosyluronic acid)-(1->4)-[2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl]-(1->4)-(3-O-benzyl-α-L-idopyranosideuronic acid) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1075217-50-3
methyl (tert-butyl 3,4-di-O-benzyl-α-L-idopyranosyluronate)-(1->4)-[2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl]-(1->4)-(tert-butyl 3-O-benzyl-α-L-idopyranosideuronate)

: 1075217-52-5
methyl (3,4-di-O-benzyl-α-L-idopyranosyluronic acid)-(1->4)-[2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl]-(1->4)-(3-O-benzyl-α-L-idopyranosideuronic acid)

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 1h;
DOI:10.1016/j.tet.2008.08.021

Reference yield: 68.0%

: 1075217-52-5
methyl (3,4-di-O-benzyl-α-L-idopyranosyluronic acid)-(1->4)-[2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl]-(1->4)-(3-O-benzyl-α-L-idopyranosideuronic acid)

: C₄₇H₄₈N₃O₂₆S₃^(5-)*5Na⁽¹⁺⁾

Guidance literature:: methyl (3,4-di-O-benzyl-α-L-idopyranosyluronic acid)-(1->4)-[2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl]-(1->4)-(3-O-benzyl-α-L-idopyranosideuronic acid); With sulfur trioxide pyridine complex; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

In methanol;
DOI:10.1016/j.tet.2008.08.021