N'-[(4-cyanophenyl)methylene]-(4-oxo-6,7-dihydro-5H-cyclopenta[4,5]thieno[2,3-d]pyrimidin-3(4H)-yl)acetohydrazone

Base Information

Chemical Name:N'-[(4-cyanophenyl)methylene]-(4-oxo-6,7-dihydro-5H-cyclopenta[4,5]thieno[2,3-d]pyrimidin-3(4H)-yl)acetohydrazone
CAS No.:1345512-60-8
Molecular Formula:C₁₉H₁₅N₅O₂S
Molecular Weight:377.426
Hs Code.:

Synonyms:N'-[(4-cyanophenyl)methylene]-(4-oxo-6,7-dihydro-5H-cyclopenta[4,5]thieno[2,3-d]pyrimidin-3(4H)-yl)acetohydrazone

Suppliers and Price of N'-[(4-cyanophenyl)methylene]-(4-oxo-6,7-dihydro-5H-cyclopenta[4,5]thieno[2,3-d]pyrimidin-3(4H)-yl)acetohydrazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N'-[(4-cyanophenyl)methylene]-(4-oxo-6,7-dihydro-5H-cyclopenta[4,5]thieno[2,3-d]pyrimidin-3(4H)-yl)acetohydrazone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N'-[(4-cyanophenyl)methylene]-(4-oxo-6,7-dihydro-5H-cyclopenta[4,5]thieno[2,3-d]pyrimidin-3(4H)-yl)acetohydrazone

There total 5 articles about N'-[(4-cyanophenyl)methylene]-(4-oxo-6,7-dihydro-5H-cyclopenta[4,5]thieno[2,3-d]pyrimidin-3(4H)-yl)acetohydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1345512-97-1
C₁₁H₁₂N₄O₂S

: 105-07-7
4-cyanobenzaldehyde

: 1345512-60-8
N'-[(4-cyanophenyl)methylene]-(4-oxo-6,7-dihydro-5H-cyclopenta[4,5]thieno[2,3-d]pyrimidin-3(4H)-yl)acetohydrazone

Guidance literature:: In butan-1-ol; at 110 ℃; for 12h;
DOI:10.1016/j.bmcl.2011.09.061

Reference yield:

: 4815-29-6
ethyl 2-amino-4H,5H,6H-cyclopentenothiophene-3-carboxylate

: 1345512-60-8
N'-[(4-cyanophenyl)methylene]-(4-oxo-6,7-dihydro-5H-cyclopenta[4,5]thieno[2,3-d]pyrimidin-3(4H)-yl)acetohydrazone

Guidance literature:: Multi-step reaction with 4 steps

1: 1.5 h / 200 °C

2: potassium carbonate / acetone / 48 h / 55 °C

3: hydrazine / ethanol / 12 h / Reflux

4: butan-1-ol / 12 h / 110 °C

With potassium carbonate; hydrazine; In ethanol; acetone; butan-1-ol;
DOI:10.1016/j.bmcl.2011.09.061

Reference yield:

: 433702-79-5
C₁₃H₁₄N₂O₃S

: 1345512-60-8
N'-[(4-cyanophenyl)methylene]-(4-oxo-6,7-dihydro-5H-cyclopenta[4,5]thieno[2,3-d]pyrimidin-3(4H)-yl)acetohydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine / ethanol / 12 h / Reflux

2: butan-1-ol / 12 h / 110 °C

With hydrazine; In ethanol; butan-1-ol;
DOI:10.1016/j.bmcl.2011.09.061