4,5-duhydro-1H-pyrrole-1,5-dicarboxylic acid, 1-(1,1-dimethylethyl) dicyclohexylamine salt

Base Information

Chemical Name:4,5-duhydro-1H-pyrrole-1,5-dicarboxylic acid, 1-(1,1-dimethylethyl) dicyclohexylamine salt
CAS No.:709031-41-4
Molecular Formula:C₁₀H₁₅NO₄*C₁₂H₂₃N
Molecular Weight:394.555
Hs Code.:

Synonyms:4,5-duhydro-1H-pyrrole-1,5-dicarboxylic acid, 1-(1,1-dimethylethyl) dicyclohexylamine salt

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Chemical Property of 4,5-duhydro-1H-pyrrole-1,5-dicarboxylic acid, 1-(1,1-dimethylethyl) dicyclohexylamine salt

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Technology Process of 4,5-duhydro-1H-pyrrole-1,5-dicarboxylic acid, 1-(1,1-dimethylethyl) dicyclohexylamine salt

There total 2 articles about 4,5-duhydro-1H-pyrrole-1,5-dicarboxylic acid, 1-(1,1-dimethylethyl) dicyclohexylamine salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 101-83-7
N-cyclohexyl-cyclohexanamine

: 709031-41-4
4,5-duhydro-1H-pyrrole-1,5-dicarboxylic acid, 1-(1,1-dimethylethyl) dicyclohexylamine salt

Guidance literature:: 4,5-dihydro-1H-pyrrole-1,5-dicarboxylic acid 1-(1,1-dimethylethyl) sodium salt; With phosphoric acid; In n-heptane; tert-butyl methyl ether; water; at 0 - 5 ℃; for 0.166667h; pH=2.5 - 3;

N-cyclohexyl-cyclohexanamine; In n-heptane; tert-butyl methyl ether; water; at 0 - 5 ℃; for 3h;

Reference yield:

: 101-83-7
N-cyclohexyl-cyclohexanamine

: 178172-26-4
(5S)-4,5-dihydro-1H-pyrrol-1,5-dicarboxylic acid [1-(1,1-dimethylethyl)] 5-ethyl ester

: 709031-41-4
4,5-duhydro-1H-pyrrole-1,5-dicarboxylic acid, 1-(1,1-dimethylethyl) dicyclohexylamine salt

Guidance literature:: (5S)-4,5-dihydro-1H-pyrrol-1,5-dicarboxylic acid [1-(1,1-dimethylethyl)] 5-ethyl ester; With sodium hydroxide;

With phosphoric acid;

N-cyclohexyl-cyclohexanamine;
DOI:10.1021/jo500966m

Reference yield:

: 709031-41-4
4,5-duhydro-1H-pyrrole-1,5-dicarboxylic acid, 1-(1,1-dimethylethyl) dicyclohexylamine salt

: 361440-67-7
[1S-(1α,3β,5α)]-3-(aminocarbonyl)-2-azabicyclo[3.1.0]hexane-2-carboxylic acid 1,1-dimethylethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / water

2.1: ammonium hydroxide / Inert atmosphere

3.1: diethylzinc / ethyl acetate; water; toluene / 105 h / -10 - 0 °C / Inert atmosphere

3.2: 1.67 h / -10 - 16 °C / Inert atmosphere

With ammonium hydroxide; diethylzinc; sodium hydroxide; In water; ethyl acetate; toluene;
DOI:10.1021/jo500966m