(5-fluoro-2-(2-(4-(trifluoromethyl)phenyl)ethynyl)phenyl)diphenylsilanol

Base Information

Chemical Name:(5-fluoro-2-(2-(4-(trifluoromethyl)phenyl)ethynyl)phenyl)diphenylsilanol
CAS No.:1388859-18-4
Molecular Formula:C₂₇H₁₈F₄OSi
Molecular Weight:462.518
Hs Code.:

Synonyms:(5-fluoro-2-(2-(4-(trifluoromethyl)phenyl)ethynyl)phenyl)diphenylsilanol

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Chemical Property of (5-fluoro-2-(2-(4-(trifluoromethyl)phenyl)ethynyl)phenyl)diphenylsilanol

Chemical Property:

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Technology Process of (5-fluoro-2-(2-(4-(trifluoromethyl)phenyl)ethynyl)phenyl)diphenylsilanol

There total 5 articles about (5-fluoro-2-(2-(4-(trifluoromethyl)phenyl)ethynyl)phenyl)diphenylsilanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₇H₁₈F₄Si

: 1388859-18-4
(5-fluoro-2-(2-(4-(trifluoromethyl)phenyl)ethynyl)phenyl)diphenylsilanol

Guidance literature:: With [RhCl₂(p-cymene)]2; In water; acetonitrile; at 80 ℃; air;
DOI:10.1021/ol301660f

Reference yield:

: 1326706-58-4
C₁₅H₇BrF₄

: 1388859-18-4
(5-fluoro-2-(2-(4-(trifluoromethyl)phenyl)ethynyl)phenyl)diphenylsilanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: [RhCl₂(p-cymene)]2 / water; acetonitrile / 80 °C / air

With n-butyllithium; [RhCl₂(p-cymene)]2; In tetrahydrofuran; hexane; water; acetonitrile;
DOI:10.1021/ol301660f

Reference yield:

: 705-31-7
4-trifluoromethylphenylacetylene

: 1388859-18-4
(5-fluoro-2-(2-(4-(trifluoromethyl)phenyl)ethynyl)phenyl)diphenylsilanol

Guidance literature:: Multi-step reaction with 3 steps

1.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

3.1: [RhCl₂(p-cymene)]2 / water; acetonitrile / 80 °C / air

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; n-butyllithium; [RhCl₂(p-cymene)]2; triethylamine; In tetrahydrofuran; hexane; water; acetonitrile;
DOI:10.1021/ol301660f