Technology Process of C25H27IN2O8
There total 6 articles about C25H27IN2O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
manganese(IV) oxide;
In
1,4-dioxane;
Reflux;
Inert atmosphere;
DOI:10.1002/ejoc.201101744
- Guidance literature:
-
Multi-step reaction with 2 steps
1: toluene / 90 °C / Inert atmosphere
2: manganese(IV) oxide / 1,4-dioxane / Reflux; Inert atmosphere
With
manganese(IV) oxide;
In
1,4-dioxane; toluene;
1: Diels-Alder reaction;
DOI:10.1002/ejoc.201101744
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sulfuric acid; iodine; acetic acid / 21 h / 70 °C / Inert atmosphere
2: thionyl chloride / 24 h / 0 - 20 °C / Inert atmosphere
3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / tetrahydrofuran / 24 h / 0 - 20 °C / pH 9 / Inert atmosphere
4: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 20 °C / 760.05 Torr
5: toluene / 90 °C / Inert atmosphere
6: manganese(IV) oxide / 1,4-dioxane / Reflux; Inert atmosphere
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; manganese(IV) oxide; thionyl chloride; sulfuric acid; iodine; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; toluene;
5: Diels-Alder reaction;
DOI:10.1002/ejoc.201101744
