(3R,4S,5R,6S)-3,6-Diacetoxy-4,5-bis-methanesulfonyloxy-cyclohex-1-enecarboxylic acid

Base Information

Chemical Name:(3R,4S,5R,6S)-3,6-Diacetoxy-4,5-bis-methanesulfonyloxy-cyclohex-1-enecarboxylic acid
CAS No.:85553-88-4
Molecular Formula:C₁₃H₁₈O₁₂S₂
Molecular Weight:430.411
Hs Code.:

Synonyms:(3R,4S,5R,6S)-3,6-Diacetoxy-4,5-bis-methanesulfonyloxy-cyclohex-1-enecarboxylic acid

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Chemical Property of (3R,4S,5R,6S)-3,6-Diacetoxy-4,5-bis-methanesulfonyloxy-cyclohex-1-enecarboxylic acid

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Technology Process of (3R,4S,5R,6S)-3,6-Diacetoxy-4,5-bis-methanesulfonyloxy-cyclohex-1-enecarboxylic acid

There total 2 articles about (3R,4S,5R,6S)-3,6-Diacetoxy-4,5-bis-methanesulfonyloxy-cyclohex-1-enecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 85553-87-3
Acetic acid (1S,4R,5S,6R)-4-acetoxy-2-formyl-5,6-bis-methanesulfonyloxy-cyclohex-2-enyl ester

: 85553-88-4
(3R,4S,5R,6S)-3,6-Diacetoxy-4,5-bis-methanesulfonyloxy-cyclohex-1-enecarboxylic acid

Guidance literature:: With chromium(VI) oxide; sulfuric acid; water; In acetone; at 0 ℃; for 0.5h;

Reference yield:

: 85553-86-2
Acetic acid (1R,4S,5S,6R)-4-acetoxy-2-formyl-5,6-dihydroxy-cyclohex-2-enyl ester

: 85553-88-4
(3R,4S,5R,6S)-3,6-Diacetoxy-4,5-bis-methanesulfonyloxy-cyclohex-1-enecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / triethylamine / CH₂Cl₂ / 0.67 h / -15 deg C to room temp.

2: 92 percent / CrO₃, H₂SO₄, H₂O / acetone / 0.5 h / 0 °C

With chromium(VI) oxide; sulfuric acid; water; triethylamine; In dichloromethane; acetone;