N-[4-(7-diethoxyphosphoryl-4,7,10,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-trienyl)-1,4-phenylenebis(methylene)]-2-(aminomethyl)pyridine

Base Information

• Chemical Name: N-[4-(7-diethoxyphosphoryl-4,7,10,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-trienyl)-1,4-phenylenebis(methylene)]-2-(aminomethyl)pyridine
• CAS No.: 255383-33-6
• Molecular Formula: C₃₁H₄₅N₆O₃P
• Molecular Weight: 580.71

Synonyms:N-[4-(7-diethoxyphosphoryl-4,7,10,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-trienyl)-1,4-phenylenebis(methylene)]-2-(aminomethyl)pyridine

Chemical Property of N-[4-(7-diethoxyphosphoryl-4,7,10,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-trienyl)-1,4-phenylenebis(methylene)]-2-(aminomethyl)pyridine

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Technology Process of N-[4-(7-diethoxyphosphoryl-4,7,10,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-trienyl)-1,4-phenylenebis(methylene)]-2-(aminomethyl)pyridine

There total 1 articles about N-[4-(7-diethoxyphosphoryl-4,7,10,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-trienyl)-1,4-phenylenebis(methylene)]-2-(aminomethyl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

N-{4-[7-diethoxyphosphoryl-10-(2-nitrobenzenesulfonyl)-4,7,10,17-tetraazabicyclo[11.3.1]heptadeca-1(17),13,15-trienyl]-1,4-phenylenebis(methylene)}-N-(2-nitrobenzenesulfonyl)-2-(aminomethyl)pyridine (255383-32-5) → N-[4-(7-diethoxyphosphoryl-4,7,10,17-tetraazabicyclo[11.3.1]heptadeca-1(17),13,15-trienyl)-1,4-phenylenebis(methylene)]-2-(aminomethyl)pyridine (255383-33-6)

Guidance literature:

With potassium carbonate; thiophenol; In N,N-dimethyl-formamide; at 50 ℃; for 15h; Inert atmosphere;

DOI:10.1021/jm901530b

Reference yield: 63.0%

N-[4-(7-diethoxyphosphoryl-4,7,10,17-tetraazabicyclo[11.3.1]heptadeca-1(17),13,15-trienyl)-1,4-phenylenebis(methylene)]-2-(aminomethyl)pyridine (255383-33-6) → N-[4-(4,7,10,17-tetraazabicyclo[11.3.1]heptadeca-1(17),13,15-trienyl)-1,4-phenylenebis(methylene)]-2-(aminomethyl)pyridine hexahydrobromide

Guidance literature:

With hydrogen bromide; In acetic acid; at 20 ℃; for 4h;

DOI:10.1021/jm901530b

upstream raw materials:

N-{4-[7-diethoxyphosphoryl-10-(2-nitrobenzenesulfonyl)-4,7,10,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-trienyl]-1,4-phenylenebis(methylene)}-N-(2-nitrobenzenesulfonyl)-2-(aminomethyl)pyridine

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