1,1'-BIS[2,4,8,10-TETRAKIS(1,1-DIMETHYLETHYL)DIBENZO[D,F][1,3,2]DIOXAPHOSPHEPIN-6-YL]FERROCENE

Base Information

Chemical Name:1,1'-BIS[2,4,8,10-TETRAKIS(1,1-DIMETHYLETHYL)DIBENZO[D,F][1,3,2]DIOXAPHOSPHEPIN-6-YL]FERROCENE
CAS No.:214151-82-3
Molecular Formula:C₆₆H₈₈FeO₄P₂
Molecular Weight:1063.22
Hs Code.:
Mol file:214151-82-3.mol

Synonyms:1,1’-BIS[2,4,8,10-TETRAKIS(1,1-DIMETHYLETHYL)DIBENZO[D,F][1,3,2]DIOXAPHOSPHEPIN-6-YL]FERROCENE;1,1’-Bis[2,4,8,10-tetrakis(1,1-dimethylethyl)dibenzo[d,f][1,3,2]dioxaphosphepin-

Suppliers and Price of 1,1'-BIS[2,4,8,10-TETRAKIS(1,1-DIMETHYLETHYL)DIBENZO[D,F][1,3,2]DIOXAPHOSPHEPIN-6-YL]FERROCENE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1,1'-BIS[2,4,8,10-TETRAKIS(1,1-DIMETHYLETHYL)DIBENZO[D,F][1,3,2]DIOXAPHOSPHEPIN-6-YL]FERROCENE 95.00%
5MG
$ 496.65

Total 5 raw suppliers

Chemical Property of 1,1'-BIS[2,4,8,10-TETRAKIS(1,1-DIMETHYLETHYL)DIBENZO[D,F][1,3,2]DIOXAPHOSPHEPIN-6-YL]FERROCENE

Chemical Property:

PSA：64.10000
LogP:19.40370

Purity/Quality:

98%Min ^*data from raw suppliers

1,1'-BIS[2,4,8,10-TETRAKIS(1,1-DIMETHYLETHYL)DIBENZO[D,F][1,3,2]DIOXAPHOSPHEPIN-6-YL]FERROCENE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,1'-BIS[2,4,8,10-TETRAKIS(1,1-DIMETHYLETHYL)DIBENZO[D,F][1,3,2]DIOXAPHOSPHEPIN-6-YL]FERROCENE

There total 1 articles about 1,1'-BIS[2,4,8,10-TETRAKIS(1,1-DIMETHYLETHYL)DIBENZO[D,F][1,3,2]DIOXAPHOSPHEPIN-6-YL]FERROCENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.7%

: 102-54-5,55404-68-7
ferrocene

: 71941-98-5
3,3',5,5'-tetra-tert-butyl-1,1'-biphenyl-2,2'-diyl phosphorochloridite

: 214151-82-3
1,1'-bis[2,4,8,10-tetrakis(1,1-dimethylethyl)dibenzo[d,f][1,3,2]dioxaphosphepin-6-yl]ferrocene

Guidance literature:: With n-butyl lithium; N,N,N',N'-tetramethylethylenediamine; In tetrahydrofuran; hexane; under N2 or Ar; hexane soln. of n-BuLi added to stirred soln. of ferrocene in hexane; stirred (20 min); TMEDA added; refluxed (2 h); THF added at ambient temp.; cooled (-40°C); THF soln. of ligand added; warmed to ambient temp.; refluxed (6 h); cooled to ambient temp.; filtered; volatiles removed in vac.; residue triturated with hexane; solid recrystd. from MeCN-THF; elem. anal.;
DOI:10.1021/ic010750p