S-(4-(3,5-dimethoxy-4-propoxybenzoyl)-7-ethoxyisoquinolin-8-yl) dimethylcarbamothioate

Base Information

Chemical Name:S-(4-(3,5-dimethoxy-4-propoxybenzoyl)-7-ethoxyisoquinolin-8-yl) dimethylcarbamothioate
CAS No.:1351593-91-3
Molecular Formula:C₂₆H₃₀N₂O₆S
Molecular Weight:498.6
Hs Code.:

Synonyms:S-(4-(3,5-dimethoxy-4-propoxybenzoyl)-7-ethoxyisoquinolin-8-yl) dimethylcarbamothioate

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Chemical Property of S-(4-(3,5-dimethoxy-4-propoxybenzoyl)-7-ethoxyisoquinolin-8-yl) dimethylcarbamothioate

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Technology Process of S-(4-(3,5-dimethoxy-4-propoxybenzoyl)-7-ethoxyisoquinolin-8-yl) dimethylcarbamothioate

There total 7 articles about S-(4-(3,5-dimethoxy-4-propoxybenzoyl)-7-ethoxyisoquinolin-8-yl) dimethylcarbamothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1351593-89-9
S-(4-(3,5-dimethoxy-4-propoxybenzyl)-7-ethoxyisoquinolin-8-yl) dimethylcarbamothioate

: 1351593-91-3
S-(4-(3,5-dimethoxy-4-propoxybenzoyl)-7-ethoxyisoquinolin-8-yl) dimethylcarbamothioate

Guidance literature:: With sodium chlorite; N-hydroxyphthalimide; In water; acetonitrile; at 85 ℃; for 6h;

Reference yield:

: 134-96-3
syringic aldehyde

: 1351593-91-3
S-(4-(3,5-dimethoxy-4-propoxybenzoyl)-7-ethoxyisoquinolin-8-yl) dimethylcarbamothioate

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / N,N-dimethyl-formamide / 10 h / 40 °C / Inert atmosphere

2: hydrogenchloride / ethanol; water / 0.33 h / 100 °C

3: sodium chlorite / N-hydroxyphthalimide / acetonitrile; water / 6 h / 85 °C

With hydrogenchloride; sodium chlorite; caesium carbonate; N-hydroxyphthalimide; In ethanol; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 492-88-6
3-ethoxysalicylaldehyde

: 1351593-91-3
S-(4-(3,5-dimethoxy-4-propoxybenzoyl)-7-ethoxyisoquinolin-8-yl) dimethylcarbamothioate

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide / water; tetrahydrofuran / 0.75 h / 4 - 20 °C / Inert atmosphere

2.1: diphenylether / 0.33 h / 240 °C / Inert atmosphere

3.1: dichloromethane / 0.08 h / 20 °C / Inert atmosphere

3.2: 20 °C

4.1: hydrogenchloride / ethanol; water / 0.33 h / 100 °C

5.1: sodium chlorite / N-hydroxyphthalimide / acetonitrile; water / 6 h / 85 °C

With hydrogenchloride; sodium chlorite; diphenylether; potassium hydroxide; N-hydroxyphthalimide; In tetrahydrofuran; ethanol; dichloromethane; water; acetonitrile;