N-phenyl-2-[3-({3-[2-(anilinothiocarbonyl)hydrazino]-3-oxopropyl}anilino)propanoyl]-1-hydrazino-carbothioamide

Base Information

Chemical Name:N-phenyl-2-[3-({3-[2-(anilinothiocarbonyl)hydrazino]-3-oxopropyl}anilino)propanoyl]-1-hydrazino-carbothioamide
CAS No.:1071781-15-1
Molecular Formula:C₂₆H₂₉N₇O₂S₂
Molecular Weight:535.694
Hs Code.:

Synonyms:N-phenyl-2-[3-({3-[2-(anilinothiocarbonyl)hydrazino]-3-oxopropyl}anilino)propanoyl]-1-hydrazino-carbothioamide

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Chemical Property of N-phenyl-2-[3-({3-[2-(anilinothiocarbonyl)hydrazino]-3-oxopropyl}anilino)propanoyl]-1-hydrazino-carbothioamide

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Technology Process of N-phenyl-2-[3-({3-[2-(anilinothiocarbonyl)hydrazino]-3-oxopropyl}anilino)propanoyl]-1-hydrazino-carbothioamide

There total 1 articles about N-phenyl-2-[3-({3-[2-(anilinothiocarbonyl)hydrazino]-3-oxopropyl}anilino)propanoyl]-1-hydrazino-carbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 56329-74-9
3,3′-(phenylazanediyl)dipropanehydrazide

: 103-72-0
phenyl isothiocyanate

: 1071781-15-1
N-phenyl-2-[3-({3-[2-(anilinothiocarbonyl)hydrazino]-3-oxopropyl}anilino)propanoyl]-1-hydrazino-carbothioamide

Guidance literature:: In methanol; for 4h; Heating;
DOI:10.1007/s10593-007-0176-9

Reference yield: 47.0%

: 1071781-15-1
N-phenyl-2-[3-({3-[2-(anilinothiocarbonyl)hydrazino]-3-oxopropyl}anilino)propanoyl]-1-hydrazino-carbothioamide

: N-phenyl-5-(2-(phenyl(2-(5-(phenylamino)-1,3,4-thiadiazol-2-yl)ethyl)amino)ethyl)-1,3,4-thiadiazol-2-amine

Guidance literature:: With sulfuric acid; at 20 ℃; for 0.25h;
DOI:10.1007/s11164-015-2290-0

Reference yield:

: 1071781-15-1
N-phenyl-2-[3-({3-[2-(anilinothiocarbonyl)hydrazino]-3-oxopropyl}anilino)propanoyl]-1-hydrazino-carbothioamide

: N,N-bis(2-(5-(ethylthio)-4-phenyl-4H-1,2,4-triazol-3-yl)ethyl)aniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / 4 h / Reflux

2.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 20 °C

2.2: 20 h / 50 °C

With sodium hydride; potassium hydroxide; In N,N-dimethyl-formamide;
DOI:10.1007/s11164-015-2290-0