[4-((3,5-bis[2-(bis(carboxymethyl)amino)ethylcarbamoyl]phenylcarbamoyl)methyl)-7,10-bis(carboxymethyl)-1,4,7,10-tetraazacyclododec-1-yl]acetic acid

Base Information

Chemical Name:[4-((3,5-bis[2-(bis(carboxymethyl)amino)ethylcarbamoyl]phenylcarbamoyl)methyl)-7,10-bis(carboxymethyl)-1,4,7,10-tetraazacyclododec-1-yl]acetic acid
CAS No.:1239340-13-6
Molecular Formula:C₃₆H₅₃N₉O₁₇
Molecular Weight:883.867
Hs Code.:

[4-((3,5-bis[2-(bis(carboxymethyl)amino)ethylcarbamoyl]phenylcarbamoyl)methyl)-7,10-bis(carboxymethyl)-1,4,7,10-tetraazacyclododec-1-yl]acetic acid

Synonyms:[4-((3,5-bis[2-(bis(carboxymethyl)amino)ethylcarbamoyl]phenylcarbamoyl)methyl)-7,10-bis(carboxymethyl)-1,4,7,10-tetraazacyclododec-1-yl]acetic acid

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Chemical Property of [4-((3,5-bis[2-(bis(carboxymethyl)amino)ethylcarbamoyl]phenylcarbamoyl)methyl)-7,10-bis(carboxymethyl)-1,4,7,10-tetraazacyclododec-1-yl]acetic acid

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Technology Process of [4-((3,5-bis[2-(bis(carboxymethyl)amino)ethylcarbamoyl]phenylcarbamoyl)methyl)-7,10-bis(carboxymethyl)-1,4,7,10-tetraazacyclododec-1-yl]acetic acid

There total 7 articles about [4-((3,5-bis[2-(bis(carboxymethyl)amino)ethylcarbamoyl]phenylcarbamoyl)methyl)-7,10-bis(carboxymethyl)-1,4,7,10-tetraazacyclododec-1-yl]acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1239340-11-4
C₆₄H₁₀₉N₉O₁₇

: 1239340-13-6
[4-((3,5-bis[2-(bis(carboxymethyl)amino)ethylcarbamoyl]phenylcarbamoyl)methyl)-7,10-bis(carboxymethyl)-1,4,7,10-tetraazacyclododec-1-yl]acetic acid

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1039/b925556g

Reference yield:

: 1239340-10-3
C₃₈H₆₀BrN₅O₁₁

: 1239340-13-6
[4-((3,5-bis[2-(bis(carboxymethyl)amino)ethylcarbamoyl]phenylcarbamoyl)methyl)-7,10-bis(carboxymethyl)-1,4,7,10-tetraazacyclododec-1-yl]acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 16 h / 70 °C

2: trifluoroacetic acid / dichloromethane / 24 h / 20 °C

With potassium carbonate; trifluoroacetic acid; In dichloromethane; acetonitrile;
DOI:10.1039/b925556g

Reference yield:

: 737820-87-0
C₁₈H₁₇NO₆

: 1239340-13-6
[4-((3,5-bis[2-(bis(carboxymethyl)amino)ethylcarbamoyl]phenylcarbamoyl)methyl)-7,10-bis(carboxymethyl)-1,4,7,10-tetraazacyclododec-1-yl]acetic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: methanol / 12 h / 20 °C

2.1: potassium carbonate / acetonitrile / 0.5 h / 20 °C

2.2: 18 h / 70 °C

3.1: palladium on carbon; hydrogen / ethanol / 24 h / 1551.49 Torr

4.1: potassium carbonate / dichloromethane / 0 °C

4.2: 0 - 20 °C

5.1: potassium carbonate / acetonitrile / 16 h / 70 °C

6.1: trifluoroacetic acid / dichloromethane / 24 h / 20 °C

With palladium on carbon; hydrogen; potassium carbonate; trifluoroacetic acid; In methanol; ethanol; dichloromethane; acetonitrile;
DOI:10.1039/b925556g