BENZYL TRANS-(6-HYDROXYMETHYL)CYCLOHEX-3-ENYLCARBAMATE

Base Information

• Chemical Name: BENZYL TRANS-(6-HYDROXYMETHYL)CYCLOHEX-3-ENYLCARBAMATE
• CAS No.: 213672-73-2
• Molecular Formula: C₁₅H₁₉NO₃
• Molecular Weight: 261.321
• Mol file: 213672-73-2.mol

Synonyms:BENZYL TRANS-(6-HYDROXYMETHYL)CYCLOHEX-3-ENYLCARBAMATE;Carbamic acid, [(1R,6R)-6-(hydroxymethyl)-3-cyclohexen-1-yl]-, phenylmethyl ester, rel- (9CI)

Chemical Property of BENZYL TRANS-(6-HYDROXYMETHYL)CYCLOHEX-3-ENYLCARBAMATE

Chemical Property:

• Vapor Pressure: 3.35E-08mmHg at 25°C
• Refractive Index: 1.574
• Boiling Point: 431.2°C at 760 mmHg
• Flash Point: 214.6°C
• PSA: 58.56000
• Density: 1.17g/cm³
• LogP: 2.63080

Purity/Quality:

99% ^*data from raw suppliers

Benzyl trans-(6-hydroxymethyl)-cyclohex-3-enylcarbamate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BENZYL TRANS-(6-HYDROXYMETHYL)CYCLOHEX-3-ENYLCARBAMATE

There total 8 articles about BENZYL TRANS-(6-HYDROXYMETHYL)CYCLOHEX-3-ENYLCARBAMATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cis-2-(hydroxymethyl)-4-cyclohexenyl-1-amine (98769-56-3,98769-57-4,191803-49-3,213672-86-7,213672-92-5,213881-14-2,213881-15-3) → ((1S,6R)-6-Hydroxymethyl-cyclohex-3-enyl)-carbamic acid benzyl ester (213672-73-2)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. Na₂CO₃ / CH₂Cl₂ / Ambient temperature

With sodium carbonate; In dichloromethane;

DOI:10.1016/S0957-4166(98)00236-5

Reference yield:

trans-2-(hydroxymethyl)-4-cyclohexenyl-1-amine (98769-56-3,98769-57-4,191803-49-3,213672-86-7,213672-92-5,213881-14-2,213881-15-3) → ((1R,6R)-6-Hydroxymethyl-cyclohex-3-enyl)-carbamic acid benzyl ester (213672-73-2)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. Na₂CO₃ / CH₂Cl₂ / Ambient temperature

With sodium carbonate; In dichloromethane;

DOI:10.1016/S0957-4166(98)00236-5

Reference yield:

benzyl chloroformate (501-53-1,94274-21-2) → ((1S,6R)-6-Hydroxymethyl-cyclohex-3-enyl)-carbamic acid benzyl ester (213672-73-2)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. Na₂CO₃ / CH₂Cl₂ / Ambient temperature

With sodium carbonate; In dichloromethane;

DOI:10.1016/S0957-4166(98)00236-5

upstream raw materials:

(1R,6S)-6-Benzyloxycarbonylamino-cyclohex-3-enecarboxylic acid

cis-2-(hydroxymethyl)-4-cyclohexenyl-1-amine

benzyl chloroformate

((1S,6R)-6-Hydroxymethyl-cyclohex-3-enyl)-carbamic acid benzyl ester

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