C₅₃H₈₈O₇Si₃

Base Information

Chemical Name:C₅₃H₈₈O₇Si₃
CAS No.:948297-31-2
Molecular Formula:C₅₃H₈₈O₇Si₃
Molecular Weight:921.534
Hs Code.:

C<sub>53</sub>H<sub>88</sub>O<sub>7</sub>Si<sub>3</sub>

Synonyms:C₅₃H₈₈O₇Si₃

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Chemical Property of C₅₃H₈₈O₇Si₃

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Technology Process of C₅₃H₈₈O₇Si₃

There total 28 articles about C₅₃H₈₈O₇Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 948297-18-5
C₁₂H₂₁NO₄

: 948297-31-2
C₅₃H₈₈O₇Si₃

Guidance literature:: Multi-step reaction with 14 steps

1.1: n-BuLi / diethyl ether / -78 °C

1.2: MgBr₂*OEt₂ / diethyl ether / -78 - 0 °C

1.3: THF / diethyl ether / 20 °C

2.1: 4-dimethylaminopyridine; pyridine / CH₂Cl₂

3.1: (S)-1-Me-3,3-diPh-tetrahydropyrrolo[1,2-c][1,3,2]oxazaborole; BH₃*SMe₂ / tetrahydrofuran / 0 °C

4.1: H₂; pyridine / Pd/CaCO₃/Pb / benzene / 760.05 Torr

4.2: 4-dimethylaminopyridine; imidazole / dimethylformamide

5.1: K₂CO₃ / methanol

6.1: SO₃*pyridine; dimethylsulfoxide; iPr₂NEt / CH₂Cl₂ / -25 °C

7.1: 74 percent / HF*pyridine; pyridine / tetrahydrofuran / 0 °C

8.1: 92 percent / pyridinium p-toluenesulfonate; HC(OMe)3 / CH₂Cl₂ / -10 °C

9.1: 88 percent / H₂O₂; [(NH₄)6Mo₇O₂₄] / methanol / 0 °C

10.1: 92 percent / LiAlH₄ / diethyl ether / -20 °C

11.1: 98 percent / imidazole / dimethylformamide

12.1: lithium diisopropylamide / tetrahydrofuran / -78 °C

13.1: Dess-Martin periodinane; pyridine / CH₂Cl₂

14.1: 92 percent / Na/Hg; NaH₂PO₄ / tetrahydrofuran; methanol / -10 °C

With pyridine; 1H-imidazole; dmap; sodium dihydrogenphosphate; sodium amalgam; lithium aluminium tetrahydride; n-butyllithium; pyridine-SO₃ complex; dimethylsulfide borane complex; hydrogen; dihydrogen peroxide; pyridinium p-toluenesulfonate; potassium carbonate; Dess-Martin periodane; pyridine hydrogenfluoride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; lithium diisopropyl amide; trimethyl orthoformate; Lindlar's catalyst; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; benzene; 3.1: Corey-Bakshi-Shibata reduction / 6.1: Parikh-Doering oxidation / 13.1: Dess-Martin oxidation;
DOI:10.1002/anie.200701515

Reference yield:

: C₂₂H₂₈O₄S

: 948297-31-2
C₅₃H₈₈O₇Si₃

Guidance literature:: Multi-step reaction with 13 steps

1.1: 4-dimethylaminopyridine; pyridine / CH₂Cl₂

2.1: (S)-1-Me-3,3-diPh-tetrahydropyrrolo[1,2-c][1,3,2]oxazaborole; BH₃*SMe₂ / tetrahydrofuran / 0 °C

3.1: H₂; pyridine / Pd/CaCO₃/Pb / benzene / 760.05 Torr

3.2: 4-dimethylaminopyridine; imidazole / dimethylformamide

4.1: K₂CO₃ / methanol

5.1: SO₃*pyridine; dimethylsulfoxide; iPr₂NEt / CH₂Cl₂ / -25 °C

6.1: 74 percent / HF*pyridine; pyridine / tetrahydrofuran / 0 °C

7.1: 92 percent / pyridinium p-toluenesulfonate; HC(OMe)3 / CH₂Cl₂ / -10 °C

8.1: 88 percent / H₂O₂; [(NH₄)6Mo₇O₂₄] / methanol / 0 °C

9.1: 92 percent / LiAlH₄ / diethyl ether / -20 °C

10.1: 98 percent / imidazole / dimethylformamide

11.1: lithium diisopropylamide / tetrahydrofuran / -78 °C

12.1: Dess-Martin periodinane; pyridine / CH₂Cl₂

13.1: 92 percent / Na/Hg; NaH₂PO₄ / tetrahydrofuran; methanol / -10 °C

With pyridine; 1H-imidazole; dmap; sodium dihydrogenphosphate; sodium amalgam; lithium aluminium tetrahydride; pyridine-SO₃ complex; dimethylsulfide borane complex; hydrogen; dihydrogen peroxide; pyridinium p-toluenesulfonate; potassium carbonate; Dess-Martin periodane; pyridine hydrogenfluoride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; lithium diisopropyl amide; trimethyl orthoformate; Lindlar's catalyst; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; benzene; 2.1: Corey-Bakshi-Shibata reduction / 5.1: Parikh-Doering oxidation / 12.1: Dess-Martin oxidation;
DOI:10.1002/anie.200701515

Reference yield:

: 948297-20-9
C₂₄H₃₂O₅S

: 948297-31-2
C₅₃H₈₈O₇Si₃

Guidance literature:: Multi-step reaction with 11 steps

1.1: H₂; pyridine / Pd/CaCO₃/Pb / benzene / 760.05 Torr

1.2: 4-dimethylaminopyridine; imidazole / dimethylformamide

2.1: K₂CO₃ / methanol

3.1: SO₃*pyridine; dimethylsulfoxide; iPr₂NEt / CH₂Cl₂ / -25 °C

4.1: 74 percent / HF*pyridine; pyridine / tetrahydrofuran / 0 °C

5.1: 92 percent / pyridinium p-toluenesulfonate; HC(OMe)3 / CH₂Cl₂ / -10 °C

6.1: 88 percent / H₂O₂; [(NH₄)6Mo₇O₂₄] / methanol / 0 °C

7.1: 92 percent / LiAlH₄ / diethyl ether / -20 °C

8.1: 98 percent / imidazole / dimethylformamide

9.1: lithium diisopropylamide / tetrahydrofuran / -78 °C

10.1: Dess-Martin periodinane; pyridine / CH₂Cl₂

11.1: 92 percent / Na/Hg; NaH₂PO₄ / tetrahydrofuran; methanol / -10 °C

With pyridine; 1H-imidazole; sodium dihydrogenphosphate; sodium amalgam; lithium aluminium tetrahydride; pyridine-SO₃ complex; hydrogen; dihydrogen peroxide; pyridinium p-toluenesulfonate; potassium carbonate; Dess-Martin periodane; pyridine hydrogenfluoride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; trimethyl orthoformate; Lindlar's catalyst; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; benzene; 3.1: Parikh-Doering oxidation / 10.1: Dess-Martin oxidation;
DOI:10.1002/anie.200701515