Acetic acid (E)-(S)-1-((1S,6R)-6-isopropenyl-1,3-dimethyl-2-oxo-cyclohex-3-enyl)-4-methyl-hexa-3,5-dienyl ester

Base Information

Chemical Name:Acetic acid (E)-(S)-1-((1S,6R)-6-isopropenyl-1,3-dimethyl-2-oxo-cyclohex-3-enyl)-4-methyl-hexa-3,5-dienyl ester
CAS No.:126202-28-6
Molecular Formula:C₂₀H₂₈O₃
Molecular Weight:316.441
Hs Code.:

Synonyms:Acetic acid (E)-(S)-1-((1S,6R)-6-isopropenyl-1,3-dimethyl-2-oxo-cyclohex-3-enyl)-4-methyl-hexa-3,5-dienyl ester

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Chemical Property of Acetic acid (E)-(S)-1-((1S,6R)-6-isopropenyl-1,3-dimethyl-2-oxo-cyclohex-3-enyl)-4-methyl-hexa-3,5-dienyl ester

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Technology Process of Acetic acid (E)-(S)-1-((1S,6R)-6-isopropenyl-1,3-dimethyl-2-oxo-cyclohex-3-enyl)-4-methyl-hexa-3,5-dienyl ester

There total 13 articles about Acetic acid (E)-(S)-1-((1S,6R)-6-isopropenyl-1,3-dimethyl-2-oxo-cyclohex-3-enyl)-4-methyl-hexa-3,5-dienyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 126202-27-5
(5R,6S)-6-((E)-(S)-1-Hydroxy-4-methyl-hexa-3,5-dienyl)-5-isopropenyl-2,6-dimethyl-cyclohex-2-enone

: 108-24-7
acetic anhydride

: 126202-28-6
Acetic acid (E)-(S)-1-((1S,6R)-6-isopropenyl-1,3-dimethyl-2-oxo-cyclohex-3-enyl)-4-methyl-hexa-3,5-dienyl ester

Guidance literature:: With dmap; triethylamine; In dichloromethane; for 18h; Ambient temperature;
DOI:10.1016/S0040-4020(01)89783-0

Reference yield: 62.0%

: 307928-71-8
Acetic acid (S)-1-((1S,6R)-6-isopropenyl-1,3-dimethyl-2-oxo-cyclohex-3-enyl)-2-(3-methyl-1,1-dioxo-2,5-dihydro-1H-1λ⁶-thiophen-2-yl)-ethyl ester

: 126202-28-6
Acetic acid (E)-(S)-1-((1S,6R)-6-isopropenyl-1,3-dimethyl-2-oxo-cyclohex-3-enyl)-4-methyl-hexa-3,5-dienyl ester

: 126244-56-2
7β-acetoxy-4,8β,13-trimethyl-19-norpodocarpa-3,12-dien-14-one

Guidance literature:: With methylene blue; In benzonitrile; at 190 ℃; for 110h;
DOI:10.1039/c39920000341

Reference yield:

: 2244-16-8,6485-40-1
(S)-p-mentha-6,8-dien-2-one

: 126202-28-6
Acetic acid (E)-(S)-1-((1S,6R)-6-isopropenyl-1,3-dimethyl-2-oxo-cyclohex-3-enyl)-4-methyl-hexa-3,5-dienyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / LDA / tetrahydrofuran / -10 °C

2: 60 percent / LDA / tetrahydrofuran / -100 °C

3: 100 percent / Et₃N, N,N-dimethylaminopyridine / CH₂Cl₂

With dmap; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c39890001294