C₆₂H₁₁₈N₂O₁₂Si₃

Base Information

Chemical Name:C₆₂H₁₁₈N₂O₁₂Si₃
CAS No.:497832-30-1
Molecular Formula:C₆₂H₁₁₈N₂O₁₂Si₃
Molecular Weight:1167.88
Hs Code.:

C<sub>62</sub>H<sub>118</sub>N<sub>2</sub>O<sub>12</sub>Si<sub>3</sub>

Synonyms:C₆₂H₁₁₈N₂O₁₂Si₃

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Chemical Property of C₆₂H₁₁₈N₂O₁₂Si₃

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Technology Process of C₆₂H₁₁₈N₂O₁₂Si₃

There total 6 articles about C₆₂H₁₁₈N₂O₁₂Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 131791-18-9
9(S)-hydroxy-6-O-methylerythromycin A

: 497832-30-1
C₆₂H₁₁₈N₂O₁₂Si₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 20 °C

2.1: lead(IV) tetraacetate / chloroform / 0.25 h / 0 °C

3.1: sodium tris(acetoxy)borohydride / chloroform / 4 h / 20 °C

4.1: sodium tris(acetoxy)borohydride / chloroform; water / 1 h / 20 °C

5.1: water; lithium hydroxide monohydrate / tetrahydrofuran; ethanol / 6 h / 20 °C

6.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran / 2 h / 20 °C

6.2: 0.5 h / Reflux

With 1H-imidazole; lithium hydroxide monohydrate; 2,4,6-trichlorobenzoyl chloride; water; lead(IV) tetraacetate; sodium tris(acetoxy)borohydride; triethylamine; In tetrahydrofuran; ethanol; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.08.007

Reference yield:

: C₆₆H₁₂₆N₂O₁₄Si₃

: 497832-30-1
C₆₂H₁₁₈N₂O₁₂Si₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium tris(acetoxy)borohydride / chloroform; water / 1 h / 20 °C

2.1: water; lithium hydroxide monohydrate / tetrahydrofuran; ethanol / 6 h / 20 °C

3.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran / 2 h / 20 °C

3.2: 0.5 h / Reflux

With lithium hydroxide monohydrate; 2,4,6-trichlorobenzoyl chloride; water; sodium tris(acetoxy)borohydride; triethylamine; In tetrahydrofuran; ethanol; chloroform; water;
DOI:10.1016/j.bmc.2012.08.007

Reference yield:

: C₅₆H₁₁₁NO₁₃Si₃

: 497832-30-1
C₆₂H₁₁₈N₂O₁₂Si₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium tris(acetoxy)borohydride / chloroform / 4 h / 20 °C

2.1: sodium tris(acetoxy)borohydride / chloroform; water / 1 h / 20 °C

3.1: water; lithium hydroxide monohydrate / tetrahydrofuran; ethanol / 6 h / 20 °C

4.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran / 2 h / 20 °C

4.2: 0.5 h / Reflux

With lithium hydroxide monohydrate; 2,4,6-trichlorobenzoyl chloride; water; sodium tris(acetoxy)borohydride; triethylamine; In tetrahydrofuran; ethanol; chloroform; water;
DOI:10.1016/j.bmc.2012.08.007