ethyl (E)-2-{5-[1-(tert-butoxycarbonyl)piperidin-4-yloxy]-2-[2-(3-cyanophenyl)ethen-1-yl]indolin-1-ylsulfonyl}acetate

Base Information

Chemical Name:ethyl (E)-2-{5-[1-(tert-butoxycarbonyl)piperidin-4-yloxy]-2-[2-(3-cyanophenyl)ethen-1-yl]indolin-1-ylsulfonyl}acetate
CAS No.:405887-30-1
Molecular Formula:C₃₁H₃₇N₃O₇S
Molecular Weight:595.717
Hs Code.:

Synonyms:ethyl (E)-2-{5-[1-(tert-butoxycarbonyl)piperidin-4-yloxy]-2-[2-(3-cyanophenyl)ethen-1-yl]indolin-1-ylsulfonyl}acetate

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Chemical Property of ethyl (E)-2-{5-[1-(tert-butoxycarbonyl)piperidin-4-yloxy]-2-[2-(3-cyanophenyl)ethen-1-yl]indolin-1-ylsulfonyl}acetate

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Technology Process of ethyl (E)-2-{5-[1-(tert-butoxycarbonyl)piperidin-4-yloxy]-2-[2-(3-cyanophenyl)ethen-1-yl]indolin-1-ylsulfonyl}acetate

There total 1 articles about ethyl (E)-2-{5-[1-(tert-butoxycarbonyl)piperidin-4-yloxy]-2-[2-(3-cyanophenyl)ethen-1-yl]indolin-1-ylsulfonyl}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 405887-29-8
tert-butyl (E)-4-{3-[4-(3-cyanophenyl)-2-hydroxy-3-buten-1-yl]-4-[(ethoxycarbonylmethylsulfonyl)amino]phenoxy}piperidine-1-carboxylate

: 405887-30-1
ethyl (E)-2-{5-[1-(tert-butoxycarbonyl)piperidin-4-yloxy]-2-[2-(3-cyanophenyl)ethen-1-yl]indolin-1-ylsulfonyl}acetate

Guidance literature:: With tributylphosphine; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1248/cpb.55.1494

Reference yield:

: 405887-30-1
ethyl (E)-2-{5-[1-(tert-butoxycarbonyl)piperidin-4-yloxy]-2-[2-(3-cyanophenyl)ethen-1-yl]indolin-1-ylsulfonyl}acetate

: 405886-59-1
C₂₆H₃₂N₄O₅S

Guidance literature:: ethyl (E)-2-{5-[1-(tert-butoxycarbonyl)piperidin-4-yloxy]-2-[2-(3-cyanophenyl)ethen-1-yl]indolin-1-ylsulfonyl}acetate; With hydrogenchloride; ethanol; In dichloromethane;

With ammonium hydroxide; ammonium chloride; In ethanol; Further stages.;
DOI:10.1248/cpb.55.1494