2-O-(p-methoxybenzyl)-3,4-O-isopropylidene-6-deoxy-6-azido-α-D-galactopyranosyl (1,1)-trichloroacetimide

Base Information

Chemical Name:2-O-(p-methoxybenzyl)-3,4-O-isopropylidene-6-deoxy-6-azido-α-D-galactopyranosyl (1,1)-trichloroacetimide
CAS No.:1176030-82-2
Molecular Formula:C₁₉H₂₃Cl₃N₄O₆
Molecular Weight:509.774
Hs Code.:

Synonyms:2-O-(p-methoxybenzyl)-3,4-O-isopropylidene-6-deoxy-6-azido-α-D-galactopyranosyl (1,1)-trichloroacetimide

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Chemical Property of 2-O-(p-methoxybenzyl)-3,4-O-isopropylidene-6-deoxy-6-azido-α-D-galactopyranosyl (1,1)-trichloroacetimide

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Technology Process of 2-O-(p-methoxybenzyl)-3,4-O-isopropylidene-6-deoxy-6-azido-α-D-galactopyranosyl (1,1)-trichloroacetimide

There total 1 articles about 2-O-(p-methoxybenzyl)-3,4-O-isopropylidene-6-deoxy-6-azido-α-D-galactopyranosyl (1,1)-trichloroacetimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: C₁₇H₂₃N₃O₆

: 545-06-2
trichloroacetonitrile

: 1176030-82-2
2-O-(p-methoxybenzyl)-3,4-O-isopropylidene-6-deoxy-6-azido-α-D-galactopyranosyl (1,1)-trichloroacetimide

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/j.tet.2009.06.007

Reference yield: 55.0%

: 1176030-82-2
2-O-(p-methoxybenzyl)-3,4-O-isopropylidene-6-deoxy-6-azido-α-D-galactopyranosyl (1,1)-trichloroacetimide

: 1176030-94-6
(2S,3S,4R)-2-(N-octanoylamino)-3,4-di-O-benzoyl-1,3,4-octadecanetriol

: 1176030-96-8
2-O-(p-methoxybenzyl)-3,4-O-isopropylidene-6-deoxy-6-azido-α-D-galactopyranosyl-(1,1)-(2S,3S,4R)-2-octanoylamino-3,4-O-dibenzoyl-octadecane-1,3,4-triol

Guidance literature:: 2-O-(p-methoxybenzyl)-3,4-O-isopropylidene-6-deoxy-6-azido-α-D-galactopyranosyl (1,1)-trichloroacetimide; (2S,3S,4R)-2-(N-octanoylamino)-3,4-di-O-benzoyl-1,3,4-octadecanetriol; In tetrahydrofuran; diethyl ether; at 20 ℃; for 0.5h; Molecular sieve;

With trimethylsilyl trifluoromethanesulfonate; In tetrahydrofuran; diethyl ether; at -25 ℃;
DOI:10.1016/j.tet.2009.06.007