C₂₃H₃₃NO₃

Base Information

Chemical Name:C₂₃H₃₃NO₃
CAS No.:1357356-14-9
Molecular Formula:C₂₃H₃₃NO₃
Molecular Weight:371.52
Hs Code.:

C<sub>23</sub>H<sub>33</sub>NO<sub>3</sub>

Synonyms:C₂₃H₃₃NO₃

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Chemical Property of C₂₃H₃₃NO₃

Chemical Property:

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Technology Process of C₂₃H₃₃NO₃

There total 6 articles about C₂₃H₃₃NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1357356-12-7
C₂₄H₃₆N₂O₄

: 917-54-4
methyllithium

: 1357356-14-9
C₂₃H₃₃NO₃

Guidance literature:: In tetrahydrofuran; diethyl ether; at -78 ℃; for 0.5h;
DOI:10.1039/c1ob06697h

Reference yield:

: C₁₇H₂₁NO₅

: 1357356-14-9
C₂₃H₃₃NO₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 - 20 °C

1.2: 2 h / -78 °C

2.1: trimethylaluminum / dichloromethane; toluene / 0.5 h / 0 °C

2.2: 3 h / 20 °C

3.1: tetrahydrofuran; diethyl ether / 0.5 h / -78 °C

With n-butyllithium; trimethylaluminum; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; toluene; 1.1: Wittig reaction / 1.2: Wittig reaction;
DOI:10.1039/c1ob06697h

Reference yield:

: 1357356-08-1
(2S,5S)-benzyl 2-(hydroxymethyl)-5-(3-methoxy-3-oxopropyl)pyrrolidine-1-carboxylate

: 1357356-14-9
C₂₃H₃₃NO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfur trioxide pyridine complex; triethylamine / dimethyl sulfoxide / 0.5 h / 0 - 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 - 20 °C

2.2: 2 h / -78 °C

3.1: trimethylaluminum / dichloromethane; toluene / 0.5 h / 0 °C

3.2: 3 h / 20 °C

4.1: tetrahydrofuran; diethyl ether / 0.5 h / -78 °C

With n-butyllithium; trimethylaluminum; sulfur trioxide pyridine complex; triethylamine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; dimethyl sulfoxide; toluene; 1.1: Parikh-Doering oxidation / 2.1: Wittig reaction / 2.2: Wittig reaction;
DOI:10.1039/c1ob06697h