1-amino-3-methylpyridin-2(1H)-iminium-2,4,6-trimethyl-benzenesulfonate

Base Information

Chemical Name:1-amino-3-methylpyridin-2(1H)-iminium-2,4,6-trimethyl-benzenesulfonate
CAS No.:1384867-92-8
Molecular Formula:C₆H₉N₃*C₉H₁₂O₃S
Molecular Weight:323.416
Hs Code.:

Synonyms:1-amino-3-methylpyridin-2(1H)-iminium-2,4,6-trimethyl-benzenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-amino-3-methylpyridin-2(1H)-iminium-2,4,6-trimethyl-benzenesulfonate

Chemical Property:

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Technology Process of 1-amino-3-methylpyridin-2(1H)-iminium-2,4,6-trimethyl-benzenesulfonate

There total 3 articles about 1-amino-3-methylpyridin-2(1H)-iminium-2,4,6-trimethyl-benzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1603-40-3
3-methylpyridin-2-ylamine

: 36016-40-7
mesitylenesulfonylhydroxylamine

: 1384867-92-8
1-amino-3-methylpyridin-2(1H)-iminium-2,4,6-trimethyl-benzenesulfonate

Guidance literature:: In dichloromethane; at 20 ℃; for 12h;

Reference yield:

: 36016-39-4
N-(tert-butoxycarbonyl)-O-(mesitylsulfonyl)hydroxylamine

: 1384867-92-8
1-amino-3-methylpyridin-2(1H)-iminium-2,4,6-trimethyl-benzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / 0.67 h / 10 °C

2: dichloromethane / 12 h / 20 °C

With trifluoroacetic acid; In dichloromethane;

Reference yield:

: 773-64-8
2-mesitylenesulphonyl chloride

: 1384867-92-8
1-amino-3-methylpyridin-2(1H)-iminium-2,4,6-trimethyl-benzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / diethyl ether / 20 °C

2: trifluoroacetic acid / 0.67 h / 10 °C

3: dichloromethane / 12 h / 20 °C

With triethylamine; trifluoroacetic acid; In diethyl ether; dichloromethane;