(1S,7R)-(+)-3-benzhydryl-10,10-dimethyl-3,4-diaza-tricyclo[5.2.1.0^1,5]dec-4-en-2-one

Base Information

• Chemical Name: (1S,7R)-(+)-3-benzhydryl-10,10-dimethyl-3,4-diaza-tricyclo[5.2.1.0^1,5]dec-4-en-2-one
• CAS No.: 1007293-19-7
• Molecular Formula: C₂₃H₂₄N₂O
• Molecular Weight: 344.456

Synonyms:(1S,7R)-(+)-3-benzhydryl-10,10-dimethyl-3,4-diaza-tricyclo[5.2.1.0^1,5]dec-4-en-2-one

Chemical Property of (1S,7R)-(+)-3-benzhydryl-10,10-dimethyl-3,4-diaza-tricyclo[5.2.1.0^1,5]dec-4-en-2-one

Chemical Property:

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Technology Process of (1S,7R)-(+)-3-benzhydryl-10,10-dimethyl-3,4-diaza-tricyclo[5.2.1.0^1,5]dec-4-en-2-one

There total 3 articles about (1S,7R)-(+)-3-benzhydryl-10,10-dimethyl-3,4-diaza-tricyclo[5.2.1.0^1,5]dec-4-en-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

(1S,4R)-(+)-2-(benzhydryl-hydrazono)-7,7-dimethyl-bicyclo[2.2.1]heptane-1-carboxylic acid → (1S,7R)-(+)-3-benzhydryl-10,10-dimethyl-3,4-diaza-tricyclo[5.2.1.01,5]dec-4-en-2-one (1007293-19-7)

Guidance literature:

In 1,3,5-trimethyl-benzene; Heating;

DOI:10.1002/adsc.200600268

Reference yield:

(1S)-(+)-ketopinic acid (464-78-8,6994-94-1,64234-14-6,40724-67-2) → (1S,7R)-(+)-3-benzhydryl-10,10-dimethyl-3,4-diaza-tricyclo[5.2.1.01,5]dec-4-en-2-one (1007293-19-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / acetic acid / CH₂Cl₂ / 22 °C

2: 62 percent / 1,3,5-trimethyl-benzene / Heating

With acetic acid; In dichloromethane; 1,3,5-trimethyl-benzene;

DOI:10.1002/adsc.200600268

Reference yield:

diphenylmethyl hydrazine (61765-84-2) → (1S,7R)-(+)-3-benzhydryl-10,10-dimethyl-3,4-diaza-tricyclo[5.2.1.01,5]dec-4-en-2-one (1007293-19-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / acetic acid / CH₂Cl₂ / 22 °C

2: 62 percent / 1,3,5-trimethyl-benzene / Heating

With acetic acid; In dichloromethane; 1,3,5-trimethyl-benzene;

DOI:10.1002/adsc.200600268

upstream raw materials:

(1S)-(+)-ketopinic acid

diphenylmethyl hydrazine

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