[1-[2-(3-azido-propyl)-oxiranyl]-1-(3-methoxy-phenyl)-ethoxy]-trimethyl-silane

Base Information

Chemical Name:[1-[2-(3-azido-propyl)-oxiranyl]-1-(3-methoxy-phenyl)-ethoxy]-trimethyl-silane
CAS No.:916753-76-9
Molecular Formula:C₁₇H₂₇N₃O₃Si
Molecular Weight:349.505
Hs Code.:

Synonyms:[1-[2-(3-azido-propyl)-oxiranyl]-1-(3-methoxy-phenyl)-ethoxy]-trimethyl-silane

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Chemical Property of [1-[2-(3-azido-propyl)-oxiranyl]-1-(3-methoxy-phenyl)-ethoxy]-trimethyl-silane

Chemical Property:

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Technology Process of [1-[2-(3-azido-propyl)-oxiranyl]-1-(3-methoxy-phenyl)-ethoxy]-trimethyl-silane

There total 7 articles about [1-[2-(3-azido-propyl)-oxiranyl]-1-(3-methoxy-phenyl)-ethoxy]-trimethyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [5-Azido-1-(3-methoxy-phenyl)-1-methyl-2-methylene-pentyloxy]-trimethyl-silane

: 916753-76-9
[1-[2-(3-azido-propyl)-oxiranyl]-1-(3-methoxy-phenyl)-ethoxy]-trimethyl-silane

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 2.5h;
DOI:10.1021/ol062116r

Reference yield:

: 916754-05-7
5-(3-methoxy-phenyl)-4-methylene-hexane-1,5-diol

: 916753-76-9
[1-[2-(3-azido-propyl)-oxiranyl]-1-(3-methoxy-phenyl)-ethoxy]-trimethyl-silane

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / CH₂Cl₂ / 0.08 h / 0 °C

2: 1.122 g / HMDS; pyridine / 0.5 h

3: NaN₃ / dimethylformamide / 48 h / 30 °C

4: 649 mg / NaHCO₃; m-CPBA / CH₂Cl₂ / 2.5 h

With pyridine; sodium azide; sodium hydrogencarbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; 1,1,1,3,3,3-hexamethyl-disilazane; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol062116r

Reference yield:

: methanesulfonic acid 4-[1-hydroxy-1-(3-methoxy-phenyl)-ethyl]-pent-4-enyl ester

: 916753-76-9
[1-[2-(3-azido-propyl)-oxiranyl]-1-(3-methoxy-phenyl)-ethoxy]-trimethyl-silane

Guidance literature:: Multi-step reaction with 3 steps

1: 1.122 g / HMDS; pyridine / 0.5 h

2: NaN₃ / dimethylformamide / 48 h / 30 °C

3: 649 mg / NaHCO₃; m-CPBA / CH₂Cl₂ / 2.5 h

With pyridine; sodium azide; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; 1,1,1,3,3,3-hexamethyl-disilazane; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol062116r