4-(N-Cyclohexyl-N-methylsulfamoyloxy)-5,6,7,8-tetrahydro-2-methylchinolin

Base Information

Chemical Name:4-(N-Cyclohexyl-N-methylsulfamoyloxy)-5,6,7,8-tetrahydro-2-methylchinolin
CAS No.:76495-37-9
Molecular Formula:C₁₇H₂₆N₂O₃S
Molecular Weight:338.471
Hs Code.:

Synonyms:4-(N-Cyclohexyl-N-methylsulfamoyloxy)-5,6,7,8-tetrahydro-2-methylchinolin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(N-Cyclohexyl-N-methylsulfamoyloxy)-5,6,7,8-tetrahydro-2-methylchinolin

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Technology Process of 4-(N-Cyclohexyl-N-methylsulfamoyloxy)-5,6,7,8-tetrahydro-2-methylchinolin

There total 2 articles about 4-(N-Cyclohexyl-N-methylsulfamoyloxy)-5,6,7,8-tetrahydro-2-methylchinolin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 18004-75-6
2-methyl-5,6,7,8-tetrahydro-quinolin-4-ol

: 83842-57-3
Chlor-N-cyclohexyl-N-methyl-sulfonamid

: 76495-37-9
4-(N-Cyclohexyl-N-methylsulfamoyloxy)-5,6,7,8-tetrahydro-2-methylchinolin

Guidance literature:: With potassium tert-butylate; In acetonitrile; at 50 - 60 ℃; for 5h;
DOI:10.1002/jlac.198219820908

Reference yield:

: 50553-62-3
2-methyl-8-methoxy-1H-quinolin-4-one

: 76495-37-9
4-(N-Cyclohexyl-N-methylsulfamoyloxy)-5,6,7,8-tetrahydro-2-methylchinolin

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / H₂ / 50 percent Ni/kieselguhr / methanol / 16 h / 120 °C / 75005.9 Torr

2: 87 percent / potassium-tert-butylate / acetonitrile / 5 h / 50 - 60 °C

With potassium tert-butylate; hydrogen; kieselguhr; nickel; In methanol; acetonitrile;
DOI:10.1002/jlac.198219820908