4-(3-butyl-2-oxoimidazolidin-1-yl)-N-(3,4,5-trimethoxy-phenyl)-benzenesulfonamide

Base Information

Chemical Name:4-(3-butyl-2-oxoimidazolidin-1-yl)-N-(3,4,5-trimethoxy-phenyl)-benzenesulfonamide
CAS No.:1422527-85-2
Molecular Formula:C₂₂H₂₉N₃O₆S
Molecular Weight:463.555
Hs Code.:

Synonyms:4-(3-butyl-2-oxoimidazolidin-1-yl)-N-(3,4,5-trimethoxy-phenyl)-benzenesulfonamide

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Chemical Property of 4-(3-butyl-2-oxoimidazolidin-1-yl)-N-(3,4,5-trimethoxy-phenyl)-benzenesulfonamide

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Technology Process of 4-(3-butyl-2-oxoimidazolidin-1-yl)-N-(3,4,5-trimethoxy-phenyl)-benzenesulfonamide

There total 5 articles about 4-(3-butyl-2-oxoimidazolidin-1-yl)-N-(3,4,5-trimethoxy-phenyl)-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 24313-88-0
3,4,5-Trimethoxyaniline

: 4-(3-butyl-2-oxoimidazolidin-1-yl)benzene-1-sulfonyl chloride

: 1422527-85-2
4-(3-butyl-2-oxoimidazolidin-1-yl)-N-(3,4,5-trimethoxy-phenyl)-benzenesulfonamide

Guidance literature:: With dmap; In acetonitrile; at 25 ℃; for 48h; Inert atmosphere;
DOI:10.1016/j.bmc.2018.09.001

Reference yield:

: 1848-69-7
1-phenylimidazolidin-2-one

: 1422527-85-2
4-(3-butyl-2-oxoimidazolidin-1-yl)-N-(3,4,5-trimethoxy-phenyl)-benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C

1.2: 20 h / 25 °C

2.1: chlorosulfonic acid / tetrachloromethane / 2 h / 0 °C

3.1: dmap / acetonitrile / 48 h / 25 °C / Inert atmosphere

With chlorosulfonic acid; dmap; sodium hydride; In tetrahydrofuran; tetrachloromethane; acetonitrile;
DOI:10.1016/j.bmc.2018.09.001

Reference yield:

: 62-53-3
aniline

: 1422527-85-2
4-(3-butyl-2-oxoimidazolidin-1-yl)-N-(3,4,5-trimethoxy-phenyl)-benzenesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: dichloromethane / 24 h / 25 °C

2.1: sodium hydride / tetrahydrofuran / 5.5 h / 0 - 25 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C

3.2: 20 h / 25 °C

4.1: chlorosulfonic acid / tetrachloromethane / 2 h / 0 °C

5.1: dmap / acetonitrile / 48 h / 25 °C / Inert atmosphere

With chlorosulfonic acid; dmap; sodium hydride; In tetrahydrofuran; tetrachloromethane; dichloromethane; acetonitrile;
DOI:10.1016/j.bmc.2018.09.001