2-Amino-6-(((benzyloxy)carbonyl)amino)hexanoic acid

Base Information

• Chemical Name: 2-Amino-6-(((benzyloxy)carbonyl)amino)hexanoic acid
• CAS No.: 25931-47-9
• Molecular Formula: C₁₄H₂₀N₂O₄
• Molecular Weight: 280.324
• NSC Number: 203803,118116
• Nikkaji Number: J1.086.096B
• Mol file: 25931-47-9.mol

Synonyms:N6-benzyloxycarbonyl-L-lysine;poly(N(epsilon)-benzyloxycarbonyl-L-lysine)

Chemical Property of 2-Amino-6-(((benzyloxy)carbonyl)amino)hexanoic acid

Chemical Property:

• Boiling Point: 499.6°Cat760mmHg
• Flash Point: 255.9°C
• PSA: 101.65000
• Density: 1.206g/cm³
• LogP: 2.58620
• Storage Temp.: −20°C
• XLogP3: -1.1
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 9
• Exact Mass: 280.14230712
• Heavy Atom Count: 20
• Complexity: 304

Purity/Quality:

99% ^*data from raw suppliers

Poly-epsilon-cbz-L-lysine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)COC(=O)NCCCCC(C(=O)O)N

Technology Process of 2-Amino-6-(((benzyloxy)carbonyl)amino)hexanoic acid

There total 46 articles about 2-Amino-6-(((benzyloxy)carbonyl)amino)hexanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

Z(OMe)-Lys(Z)-OH (42533-12-0) → N6-[(benzyloxy)carbonyl]-L-lysine (1155-64-2,57705-97-2,67178-46-5,25931-47-9)

Guidance literature:

With methanesulfonic acid; 3-methyl-phenol; In dichloromethane; at 25 ℃; for 0.5h;

DOI:10.1248/cpb.41.954

Reference yield: 93.0%

Copper(II); (S)-2-amino-6-benzyloxycarbonylamino-hexanoate → N6-[(benzyloxy)carbonyl]-L-lysine (1155-64-2,57705-97-2,67178-46-5,25931-47-9)

Guidance literature:

With sodium sulfide; In water; at 25 - 30 ℃; for 0.166667h;

DOI:10.1016/j.tetlet.2006.05.069

Reference yield: 90.0%

→ N6-[(benzyloxy)carbonyl]-L-lysine (1155-64-2,57705-97-2,67178-46-5,25931-47-9)

Guidance literature:

With N,N-Dibutyl-N'-(benzoyl)thioharnstoff; In ethanol; for 2h; Heating;

upstream raw materials:

2,6-diaminocaproic acid

L-lysine

N-(benzyloxycarbonyl)piperidine

L-Lysine hydrochloride

Downstream raw materials:

N⁶-benzyloxycarbonyl-N²-propionyl-lysine

N⁶-benzyloxycarbonyl-N²-butyryl-lysine

N⁶-benzyloxycarbonyl-N²-valeryl-lysine

N⁶-benzyloxycarbonyl-N²-chloroacetyl-lysine

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