C₃₅H₄₆F₂N₆O₅Si

Base Information

Chemical Name:C₃₅H₄₆F₂N₆O₅Si
CAS No.:1202760-79-9
Molecular Formula:C₃₅H₄₆F₂N₆O₅Si
Molecular Weight:696.87
Hs Code.:

C<sub>35</sub>H<sub>46</sub>F<sub>2</sub>N<sub>6</sub>O<sub>5</sub>Si

Synonyms:C₃₅H₄₆F₂N₆O₅Si

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Chemical Property of C₃₅H₄₆F₂N₆O₅Si

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Technology Process of C₃₅H₄₆F₂N₆O₅Si

There total 13 articles about C₃₅H₄₆F₂N₆O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.4%

: 1202760-77-7
C₃₂H₄₄F₂N₆O₄Si

: 814-68-6,25189-84-8
acryloyl chloride

: 1202760-79-9
C₃₅H₄₆F₂N₆O₅Si

Guidance literature:: C₃₂H₄₄F₂N₆O₄Si; With di-tert-butyl dicarbonate; In 1-methyl-pyrrolidin-2-one; at 20 ℃; for 1h;

acryloyl chloride; With potassium carbonate; In 1-methyl-pyrrolidin-2-one; at 0 ℃; for 1.5h;

Reference yield:

: 40216-83-9
L-4-hydroxyproline methyl ester hydrochloride

: 1202760-79-9
C₃₅H₄₆F₂N₆O₅Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: triethylamine / dichloromethane / 5 h / 20 °C

2.1: 1H-imidazole / N,N-dimethyl-formamide / 16 h

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.25 h / -20 °C

4.1: di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

5.1: hydrogen / palladium on activated carbon / methanol / 16 h / 20 °C

6.1: caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / palladium diacetate / toluene / 16 h / 110 °C / Inert atmosphere

7.1: hydrogen / palladium on activated carbon / methanol / 16 h / 20 °C

8.1: di-tert-butyl dicarbonate / 1-methyl-pyrrolidin-2-one / 1 h / 20 °C

8.2: 1.5 h / 0 °C

With 1H-imidazole; lithium aluminium tetrahydride; di-tert-butyl dicarbonate; di-isopropyl azodicarboxylate; hydrogen; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; triphenylphosphine; palladium on activated carbon; palladium diacetate; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1202760-79-9
C₃₅H₄₆F₂N₆O₅Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: triethylamine / dichloromethane / 5 h / 20 °C

2.1: 1H-imidazole / N,N-dimethyl-formamide / 16 h

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.25 h / -20 °C

4.1: di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

5.1: hydrogen / palladium on activated carbon / methanol / 16 h / 20 °C

6.1: caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / palladium diacetate / toluene / 16 h / 110 °C / Inert atmosphere

7.1: hydrogen / palladium on activated carbon / methanol / 16 h / 20 °C

8.1: di-tert-butyl dicarbonate / 1-methyl-pyrrolidin-2-one / 1 h / 20 °C

8.2: 1.5 h / 0 °C

With 1H-imidazole; lithium aluminium tetrahydride; di-tert-butyl dicarbonate; di-isopropyl azodicarboxylate; hydrogen; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; triphenylphosphine; palladium on activated carbon; palladium diacetate; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;